Standard operating procedure for the analysis of major ions in hydrothermal fluids by ion chromatography [version 3; peer review: 2 approved, 1 approved with reservations]

Autor: Angelina Cordone, Mustafa Yucel, Donato Giovannelli, Monica Correggia, Alessia Benedicta Bastianoni, Luciano Di Iorio
Jazyk: angličtina
Rok vydání: 2024
Předmět:
Zdroj: Open Research Europe, Vol 3 (2024)
Druh dokumentu: article
ISSN: 2732-5121
DOI: 10.12688/openreseurope.15605.3
Popis: This standard operating procedure (SOP) describes an ion chromatography (IC) procedure for the major cations and anions in hydrothermal fluids. Hydrothermal fluids are aqueous solutions with a wide range of temperature, salinity, pH and ion species that can be used by microbial metabolism as electron donors and electron acceptors. Due to the high variability of the environmental physical-chemical parameters in these samples, we have developed this protocol taking into account the special features of the matrices analyzed. An Eco IC Metrohm system equipped with a conductivity detector was used. Calibration curves are linear in the 0.1 to 10 mg/L concentration range for cations Ca2+, Na+, K+, Mg2+, NH4 + and anions Cl-, Br-, NO3 -, NO2 -, SO4 2- , PO4 3-.
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