DEVELOPING METHOD OF DIFFERENTIAL PULSE POLAROGRAPHIC FOR ANALYSIS OF CHLORAMPHENICOL RESIDUE IN MILK

Autor: Daryono Hadi Tjahjono, Amir Musadad, Septy Mariana K
Jazyk: angličtina
Rok vydání: 2010
Předmět:
Zdroj: Indonesian Journal of Chemistry, Vol 4, Iss 1, Pp 43-48 (2010)
Druh dokumentu: article
ISSN: 1411-9420
2460-1578
DOI: 10.22146/ijc.21872
Popis: A differential pulse polarographic method for a quantitative analysis of chloramphenicol residue in milk had been developed. Result showed that the method using dropping mercury electrode as working electrode, Ag/AgCl electrode as reference electrode, and platinum electrode as auxiliary electrode with an acetic buffer solution of pH 4.7 as supporting electrolyte had a recovery for chloramphenicol of (96.88 ± 3.17)% with a detection limit of 0,027 µg/mL, a quantitation limit of 0,089 µg/mL, and a determination limit of 0,010 µg/mL. Keywords: differential pulse polarography, residue, chloramphenicol, milk
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