2-(5-Iodo-2-oxoindolin-3-ylidene)hydrazinecarbothioamide including an unknown solvate

Autor:	Conceição Duarte de Bittencourt, Maciel Velasques J, Carratu Gervini, Jussiane Zambiazi P, Rosa de Menezes Vicenti J
Jazyk:	angličtina
Rok vydání:	2014
Předmět:	Hydrogen bond Thio General Chemistry Condensed Matter Physics Bioinformatics Ring (chemistry) Organic Papers Solvent Crystal lcsh:Chemistry Crystallography chemistry.chemical_compound chemistry lcsh:QD1-999 Amide General Materials Science
Zdroj:	Acta Crystallographica Section E, Vol 70, Iss 6, Pp o666-o667 (2014) Acta Crystallographica Section E: Structure Reports
ISSN:	1600-5368
Popis:	The molecule of the title compound, C9H7IN4OS, is almost planar (r.m.s. deviation = 0.0373 Å). In the molecule, N—H...N and N—H...O hydrogen bonds generate, respectively,S(5) andS(6) ring motifs. In the crystal, molecules are linkedviaN—H...O hydrogen bonds, forming chains propagating along [010]. These chains are linkedviaS...I contacts [3.4915 (16) Å], forming sheets lying parallel to (100). A region of disordered electron density, probably a disordered tetrahydrofuran solvent molecule, was treated using the SQUEEZE routine inPLATON[Spek (2009).Acta Cryst.D65, 148–155]. The formula mass and unit-cell characteristics were not taken into account during refinement.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::fd168ec479ee63c11f005186a8e3c07a http://scripts.iucr.org/cgi-bin/paper?S1600536814010782 Zobrazit plný text záznamu