Synthesis of SnSb2Te4 Microplatelets by High-energy Ball Milling
Autor: | Fernando Pacheco Tofanello, Murilo Senhuki Esposto, B. Ferreira, Mario S. da Luz, Carlos Alberto Moreira dos Santos, Ariana de Campos |
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Jazyk: | angličtina |
Rok vydání: | 2015 |
Předmět: |
Materials science
Annealing (metallurgy) Scanning electron microscope business.industry Mechanical Engineering Metallurgy semiconductors Raw material Condensed Matter Physics mechanical alloying Semiconductor Electrical resistance and conductance Chemical engineering Mechanics of Materials electrical properties TA401-492 General Materials Science Ion milling machine business Ball mill Materials of engineering and construction. Mechanics of materials Powder diffraction |
Zdroj: | Materials Research, Volume: 18, Issue: 5, Pages: 953-956, Published: OCT 2015 Materials Research v.18 n.5 2015 Materials research (São Carlos. Online) Universidade Federal de São Carlos (UFSCAR) instacron:ABM ABC ABPOL Materials Research, Vol 18, Iss 5, Pp 953-956 (2015) |
Popis: | In this work we demonstrate that high-energy ball milling process can be used to synthesize SnSb2Te4 without surfactant and further annealing. Milling parameters such as ball to raw material ratio (5:1) and milling time (2h) were determined to be suitable for synthesizing microplatelets of SnSb2Te4. The powders after milling for various durations were characterized by X-ray powder diffraction, scanning electron microscopy and electrical resistance measurements. |
Databáze: | OpenAIRE |
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