Loading of AgNPs onto the surface of boron nitride nanosheets for determination of scopoletin in Atractylodes macrocephala
| Autor: | Li Zeng, Wu Bensheng, Yinzi Yue, Shuai Yan, Xiaopeng Wang, Mingming Sun, Lianlin Su |
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| Jazyk: | angličtina |
| Rok vydání: | 2019 |
| Předmět: |
0301 basic medicine
Boron Compounds Materials science Silver Phytochemicals lcsh:Medicine Silver nanoparticle Article 03 medical and health sciences chemistry.chemical_compound 0302 clinical medicine Scopoletin lcsh:Science Electrodes Nanosheet Detection limit Multidisciplinary Nanocomposite lcsh:R Reproducibility of Results Atractylodes Electrochemical Techniques Nanostructures 030104 developmental biology chemistry Boron nitride Electrode Surface modification lcsh:Q 030217 neurology & neurosurgery Nuclear chemistry |
| Zdroj: | Scientific Reports, Vol 9, Iss 1, Pp 1-8 (2019) Scientific Reports |
| ISSN: | 2045-2322 |
| DOI: | 10.1038/s41598-019-40511-y |
| Popis: | In this work, silver nanoparticles prepared by a molten salt method were deposited onto the surface of hexagonal boron nitride nanosheet (NS/AgNP) to from a composite. The synthesized nanocomposite was applied for surface modification of screen-printed electrode (SPE). The modified electrode showed a superior performance for electrochemical detection of scopoletin. The electrochemical behaviour of NS/AgNP/SPE was studied in detail. An electrocatalytic oxidation was observed and used for analytical determination of scopoletin concentration. The response of the proposed electrochemical sensing platform was linear over a wide detection range of 2 μM to 0.45 mM with a low limit of detection (LOD) of 0.89 μM. The NS/AgNP/SPE also showed excellent reproducibility and anti-interference property. In addition, the proposed scopoletin sensor was successfully used for the determination of scopoletin in Atractylodes macrocephala herb samples. |
| Databáze: | OpenAIRE |
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