Preparation of anatase phase titanium dioxide film by non-aqueous electrodeposition
| Autor: | Tetsuya Osaka, Tokihiko Yokoshima, Kazuaki Shi, Nakajima Noriko, Masahiro Yoshino, Atsushi Sugiyama, Takuma Hachisu, Shigeki Kuroiwa |
|---|---|
| Rok vydání: | 2016 |
| Předmět: |
Anatase
Aqueous solution Materials science Annealing (metallurgy) Inorganic chemistry chemistry.chemical_element 02 engineering and technology 010402 general chemistry 021001 nanoscience & nanotechnology 01 natural sciences 0104 chemical sciences lcsh:Chemistry chemistry.chemical_compound lcsh:Industrial electrochemistry lcsh:QD1-999 chemistry Chemical engineering Titanium dioxide Sodium sulfate Electrochemistry Photocatalysis Thin film 0210 nano-technology lcsh:TP250-261 Titanium |
| Zdroj: | Electrochemistry Communications, Vol 65, Iss, Pp 5-8 (2016) |
| ISSN: | 1388-2481 |
| DOI: | 10.1016/j.elecom.2016.01.014 |
| Popis: | The electrodeposition–annealing route to fabricating thin film of the promising photocatalyst material anatase-titanium dioxide (anatase-TiO2) has been studied. The sample was deposited with a solution of N,N-dimethylformamide containing titanium compound by controlled-potential technique. SEM image showed the annealed sample at 600 °C for 1 h under air provided a continuous film with a thickness of ca. 350 nm. In this sample, X-ray photoelectron spectrum corresponding to the Ti 2p peak assigned to a chemical bond of TiO2 and X-ray diffraction peaks assigned to the anatase phase were observed, respectively. Electrochemical oxidation in sodium sulfate solution on this annealed film was enhanced in the presence of UV light radiation. These results confirm the successful synthesis of photocatalytic anatase-TiO2 film by the electrodeposition and annealing process. Keywords: Anatase-TiO2, Electrodeposition, Non-aqueous, Photosensitized electrolytic oxidation, Photocatalyst |
| Databáze: | OpenAIRE |
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