The addition of nanostructured hydroxyapatite to an experimental adhesive resin
| Autor: | C.P. Bergmann, Daniela Guerra Andrioli, Rafael Mello Trommer, Fabrício Mezzomo Collares, Vicente Castelo Branco Leitune, Susana Maria Werner Samuel |
|---|---|
| Rok vydání: | 2013 |
| Předmět: |
Dental Stress Analysis
Photoinitiators Dental Dentine-bonding agents Materials science Surface Properties Scanning electron microscope Dental bonding Statistics Nonparametric Polyethylene Glycols Polymerization Hydroxyapatite Mice Polymethacrylic Acids Flexural strength Hardness Materials Testing para-Aminobenzoates Animals Bisphenol A-Glycidyl Methacrylate Composite material Pliability General Dentistry Softening Light-Curing of Dental Adhesives Analysis of Variance Dentistry(all) Terpenes Bond strength Dental Bonding 3T3 Cells Dentine bonding agents Resin Cements Nanostructures Radiography Durapatite Solubility Dentin-Bonding Agents Methacrylates Adhesive Particle size Shear Strength |
| Zdroj: | Journal of Dentistry. 41:321-327 |
| ISSN: | 0300-5712 |
| DOI: | 10.1016/j.jdent.2013.01.001 |
| Popis: | ObjectivesWas produced nanostructured hydroxyapatite (HAnano) and evaluated the influence of its incorporation in an adhesive resin.MethodsHAnano was produced by a flame-based process and was characterized by scanning electron microscopy. The surface area, particle size, micro-Raman and cytotoxicity were evaluated. The organic phase was formulated by mixing 50wt.% Bis-GMA, 25wt.% TEGDMA, and 25wt.% HEMA. HAnano was added at seven different concentrations: 0; 0.5; 1; 2; 5; 10 and 20wt.%. Adhesive resins with hydroxyapatite incorporation were evaluated for their radiopacity, degree of conversion, flexural strength, softening in solvent and microshear bond strength. The data were analyzed by one-way ANOVA and Tukey's post hoc test (α=0.05), except for softening in solvent (paired t-test) and cytotoxicity (two-way ANOVA and Bonferroni).ResultsHAnano presented 15.096m2/g of specific surface area and a mean size of 26.7nm. The radiopacity values were not different from those of 1-mm aluminium. The degree of conversion ranged from 52.2 to 63.8%. The incorporation of HAnano did not influence the flexural strength, which ranged from 123.3 to 143.4MPa. The percentage of reduction of the microhardness after immersion in the solvent became lower as the HAnano concentration increased. The addition of 2% nanostructured hydroxyapatite resulted in a higher value of microshear bond strength than the control group (p |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|
Full Text from ScienceDirect