Spectroscopic study of carbon nitride nanoparticles synthesised by laser pyrolysis
| Autor: | E. Marino, B. Bouchet-Fabre, Cécile Reynaud, Dominique Porterat |
|---|---|
| Přispěvatelé: | Laboratoire Francis PERRIN (LFP - URA 2453), Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Institut de Chimie du CNRS (INC)-Centre National de la Recherche Scientifique (CNRS) |
| Rok vydání: | 2005 |
| Předmět: |
Laser pyrolysis
Infrared Analytical chemistry chemistry.chemical_element Infrared spectroscopy 02 engineering and technology 01 natural sciences NEXAFS chemistry.chemical_compound 0103 physical sciences Materials Chemistry Electrical and Electronic Engineering Fourier transform infrared spectroscopy Carbon nitride 010302 applied physics Extended X-ray absorption fine structure Mechanical Engineering General Chemistry Carbon nitrides 021001 nanoscience & nanotechnology Nitrogen XANES 3. Good health Electronic Optical and Magnetic Materials FT-IR [CHIM.THEO]Chemical Sciences/Theoretical and/or physical chemistry chemistry 0210 nano-technology Pyrolysis Nanopowders |
| Zdroj: | Diamond and Related Materials Diamond and Related Materials, Elsevier, 2005, 14, pp.1120-1125. ⟨10.1016/j.diamond.2004.11.007⟩ Diamond and Related Materials, 2005, 14, pp.1120-1125. ⟨10.1016/j.diamond.2004.11.007⟩ |
| ISSN: | 0925-9635 |
| DOI: | 10.1016/j.diamond.2004.11.007 |
| Popis: | The spectroscopic study of carbon nitride nanopowders elaborated by laser pyrolysis is reported. The bonding structure was determined using Infrared analysis and Near Edge X-ray Absorption Fine Structure results and the nanotexture followed by electron microscopy The different characterisation methods point out a nitrogen incorporation between 2 and 20%. Furthermore we note an evolution of the carbon nitrogen bonding type and of the electronic structure of the powders with the nitrogen concentration. A good correlation is observed between the evolution of the π* electron states as calculated from NEXAFS and the evolution of the bonding configuration revealed by the Infrared spectra. |
| Databáze: | OpenAIRE |
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