Guidelines to correctly measure the lithium ion conductivity of oxide ceramic electrolytes based on a harmonized testing procedure
Autor: | Marius Müller, Henry Auer, Alexander Bauer, Sven Uhlenbruck, Martin Finsterbusch, Katja Wätzig, Kristian Nikolowski, Sebastian Dierickx, Dina Fattakhova-Rohlfing, Olivier Guillon, André Weber |
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Přispěvatelé: | Publica |
Jazyk: | angličtina |
Rok vydání: | 2022 |
Předmět: |
round robin test
Renewable Energy Sustainability and the Environment harmonized testing procedure ionic conductivity determination impedance measurements Energy Engineering and Power Technology ceramic solid electrolytes Electrical and Electronic Engineering Physical and Theoretical Chemistry ddc:620 Engineering & allied operations |
Zdroj: | Journal of Power Sources, 531, Art.-Nr.: 231323 |
ISSN: | 0378-7753 1873-2755 |
Popis: | Ionic conductivities of Li-ion conducting ceramic electrolytes, mostly evaluated by means of impedance spectroscopy, are a key parameter decisive for their application. Nevertheless, significant deviations in the ionic conductivity of nominally identical samples are reported in literature, which are attributed to material and sample preparation as well as measurement related differences. The goal of this study is a detailed assessment of impedance measurement deviations of 10 identically prepared samples of each Li6.45La3Zr1.6Ta0.4Al0.05O12 (LLZO:Ta:Al) and Li1.3Al0.3Ti1.7(PO4)3 (LATP), respectively. By introducing a harmonized testing procedure for impedance measurement and data analysis, deviations among the participating labs were reduced to differences |
Databáze: | OpenAIRE |
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