High-pressure generation using double stage micro-paired diamond anvils shaped by focused ion beam
Autor: | Takehiko Yagi, Tetsuo Irifune, Takayuki Asakawa, Takashi Kanemura, Naohisa Hirao, Yuya Suzuki, Yasuo Ohishi, Yasushi Kuroda, Takeshi Sakai, Hiroaki Ohfuji |
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Rok vydání: | 2015 |
Předmět: | |
Zdroj: | Review of Scientific Instruments. 86:033905 |
ISSN: | 1089-7623 0034-6748 |
DOI: | 10.1063/1.4914844 |
Popis: | Micron-sized diamond anvils with a 3 μm culet were successfully processed using a focused ion beam (FIB) system and the generation of high pressures was confirmed using the double stage diamond anvil cell technique. The difficulty of aligning two second-stage micro-anvils was solved via the paired micro-anvil method. Micro-manufacturing using a FIB system enables us to control anvil shape, process any materials, including nano-polycrystalline diamond and single crystal diamond, and assemble the sample exactly in a very small space between the second-stage anvils. This method is highly reproducible. High pressures over 300 GPa were achieved, and the pressure distribution around the micro-anvil culet was evaluated by using a well-focused synchrotron micro-X-ray beam. |
Databáze: | OpenAIRE |
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