Titanium dioxide nanotubes addition to self-adhesive resin cement: Effect on physical and biological properties
Autor: | Rodrigo Cardoso de Oliveira, José Henrique Rubo, Adilson Yoshio Furuse, Cintia Kazuko Tokuhara, Larisa B. Arruda, Ana Flávia Sanches Borges, Paulo Noronha Lisboa-Filho, Carla Müller Ramos-Tonello |
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Přispěvatelé: | Universidade de São Paulo (USP), Universidade Estadual Paulista (Unesp) |
Jazyk: | angličtina |
Rok vydání: | 2017 |
Předmět: |
Materials science
Time Factors Surface Properties chemistry.chemical_element Dental Cements 02 engineering and technology Polymerization 03 medical and health sciences chemistry.chemical_compound 0302 clinical medicine Flexural strength CIMENTO RESINOSO Dental cement Materials Testing Humans Nanotechnology General Materials Science Solubility Composite material General Dentistry Curing (chemistry) Cement Titanium Nanotubes Dental cements technology industry and agriculture Dental Bonding 030206 dentistry 021001 nanoscience & nanotechnology Mechanical phenomena Resin Cements chemistry Mechanics of Materials Titanium dioxide Knoop hardness test Physical and chemical properties 0210 nano-technology |
Zdroj: | Web of Science Repositório Institucional da UNESP Universidade Estadual Paulista (UNESP) instacron:UNESP Repositório Institucional da USP (Biblioteca Digital da Produção Intelectual) Universidade de São Paulo (USP) instacron:USP |
Popis: | Made available in DSpace on 2018-11-26T17:35:10Z (GMT). No. of bitstreams: 0 Previous issue date: 2017-07-01 Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP) Objectives. This study has investigated the influence of Titanium dioxide nanotubes (TiO2-nt) addition to self-adhesive resin cement on the degree of conversion, water sorption, and water solubility, mechanical and biological properties. Methods. A commercially available auto-adhesive resin cement (RelyX U200(TM), 3M ESPE) was reinforced with varying amounts of nanotubes (0.3, 0.6, 0.9 wt%) and evaluated at different curing modes (self- and dual cure). The DC in different times (3, 6, 9, 12 and 15 min), water sorption (Ws) and solubility (Sl), 3-point flexural strength (sf), elastic modulus (E), Knoop microhardness (H) and viability of NIH/3T3 fibroblasts were performed to characterize the resin cement. Results. Reinforced self-adhesive resin cement, regardless of concentration, increased the DC for the self- and dual-curing modes at all times studied. The concentration of the TiO2-nt and the curing mode did not influence the Ws and Sl. Regarding sf, concentrations of both 0.3 and 0.9 wt% for self-curing mode resulted in data similar to that of dual-curing unreinforced cement. The E increased with the addition of 0.9 wt% for self-cure mode and H increased with 0.6 and 0.9 wt% for both curing modes. Cytotoxicity assays revealed that reinforced cements were biocompatible. Significance. TiO2-nt reinforced self-adhesive resin cement are promising materials for use in indirect dental restorations. Taken together, self-adhesive resin cement reinforced with TiO2-nt exhibited physicochemical and mechanical properties superior to those of unreinforced cements, without compromising their cellular viability. (C) 2017 The Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved. Univ Sao Paulo, Bauru Sch Dent, Dept Dent Endodont & Dent Mat, Bauru, SP, Brazil State Univ Sao Paulo, Dept Phys, Fac Sci, Bauru, SP, Brazil Univ Sao Paulo, Bauru Sch Dent, Dept Biol Sci, Bauru, SP, Brazil Univ Sao Paulo, Bauru Sch Dent, Dept Prosthodont, Bauru, SP, Brazil State Univ Sao Paulo, Dept Phys, Fac Sci, Bauru, SP, Brazil FAPESP: 2013/10021-5 |
Databáze: | OpenAIRE |
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