Hydrogen-Free Liquid-Helium Recovery Plants: The Solution for Low-Temperature Flow Impedance Blocking
| Autor: | N. Dittmar, C. Haberstroh, F. Galli, Agustín Camón, Javier Sesé, Stefano Spagna, E. Guerrero, G. Rayner, J. Sloan, W.J. van der Geest, M. Gabal, A. Fernandes, M.P. Lozano, Conrado Rillo, A. Oca, Maria Pilar Pina, F. Grau, M. Castrillo, Ana B. Arauzo, Jost Diederichs |
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| Přispěvatelé: | Ministerio de Economía y Competitividad (España), European Commission |
| Rok vydání: | 2016 |
| Předmět: |
Materials science
Hydrogen Flow impedance Liquid helium Capillary action Nuclear engineering Hydrogen molecule General Physics and Astronomy chemistry.chemical_element ComputingMilieux_LEGALASPECTSOFCOMPUTING 02 engineering and technology 021001 nanoscience & nanotechnology 01 natural sciences Blocking (computing) law.invention chemistry law Data_GENERAL 0103 physical sciences 010306 general physics 0210 nano-technology Helium ComputingMilieux_MISCELLANEOUS |
| Zdroj: | Zaguán. Repositorio Digital de la Universidad de Zaragoza instname Physical Review Applied Digital.CSIC. Repositorio Institucional del CSIC Physical Review Applied, 6, 024017 |
| Popis: | Under the terms of the Creative Commons Attribution license.-- et al. The blocking of fine-capillary tubes used as flow impedances in He4 evaporation cryostats to achieve temperatures below 4.2 K is generally attributed to nitrogen or air impurities entering these tubes from the main bath. The failure of even the most rigorous low-temperature laboratory best practices aimed at eliminating the problem by maintaining the cleanliness of the helium bath and preventing impurities from entering the capillary tubes suggests that a different cause is responsible for the inexplicable reduction of impedance flow. Many low-temperature research laboratories around the world have suffered this nuisance at a considerable financial cost due to the fact that the affected systems have to be warmed to room temperature in order to recover their normal low-temperature operation performance. Here, we propose an underlying physical mechanism responsible for the blockages based upon the freezing of molecular H2 traces present in the liquid-helium bath. Solid H2 accumulates at the impedance low-pressure side, and, after some time, it produces a total impedance blockage. The presence of H2 traces is unavoidable due its occurrence in the natural gas wells where helium is harvested, forcing gas suppliers to specify a lower bound for impurity levels at about 100 ppb even in high-grade helium. In this paper, we present a simple apparatus to detect hydrogen traces present in liquid helium and easily check the quality of the liquid. Finally, we propose a solution to eliminate the hydrogen impurities in small- and large-scale helium recovery plants. The solution has been implemented in several laboratories that previously experienced a chronic occurrence of blocking, eliminating similar occurrences for more than one year. The authors are greatly appreciative and acknowledge the financial support from the Spanish Ministry of Economy and Competitiveness through the INNPACTO Projects No. IPT-2012-0442-420000 and No. MAT2015-64083-R, in addition to European Union FEDER funds. |
| Databáze: | OpenAIRE |
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