Heating stability, physical and chemical analysis of calcium silicate‐based endodontic sealers
| Autor: | A. C. P. Janini, Gabriel Flores Abuna, Marina Angélica Marciano, E. M. Paiva, Lauter Eston Pelepenko, Thiago Bessa Marconato Antunes, Adriana de-Jesus-Soares, I. M. Raimundo, Mário Alexandre Coelho Sinhoreti, Brenda Paula Figueiredo de Almeida Gomes |
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| Rok vydání: | 2021 |
| Předmět: |
Materials science
Absorption of water Scanning electron microscope Root canal 0206 medical engineering Energy-dispersive X-ray spectroscopy Infrared spectroscopy 02 engineering and technology Heating Root Canal Filling Materials 03 medical and health sciences chemistry.chemical_compound 0302 clinical medicine Materials Testing Spectroscopy Fourier Transform Infrared medicine Humans Solubility General Dentistry Epoxy Resins Silicates 030206 dentistry Calcium Compounds 020601 biomedical engineering Silicate medicine.anatomical_structure chemistry Calcium silicate Nuclear chemistry |
| Zdroj: | International Endodontic Journal. 54:1175-1188 |
| ISSN: | 1365-2591 0143-2885 |
| DOI: | 10.1111/iej.13496 |
| Popis: | AIM To evaluate possible modifications in root canal sealers subjected to a variety of heating conditions using vibrational spectroscopy and analysis of physical and chemical properties. METHODOLOGY EndoSequence BC Sealer HiFlow, Bio-C Sealer, BioRoot RCS and AH Plus were analysed chemically using Raman spectroscopy (25-220 °C) and Fourier-transform infrared spectroscopy (FT-IR) (37-100 °C ). For FT-IR, the materials were tested individually and mixed with root dentine powder. Scanning electron microscopy (SEM) and coupled energy dispersive spectroscopy (EDS) were used to evaluate surface and chemical elements. ISO 6876-2012 and ASTM-C266-07 specifications were followed to evaluate flow, setting time (moist and dry), solubility and radiopacity. Also, pH analysis at 37 and 100 °C was performed. Shapiro-Wilk and Mixed ANOVA (within and between the effects of the subjects), Levene, and a post hoc analyses with Bonferroni correction were performed (P |
| Databáze: | OpenAIRE |
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