Spectrophotometric Determination of Tetramine in Carnivorous Gastropods with Tetrabromophenolphthalein Ethyl Ester
Autor: | Kouki Tanaka, Etsuo Mori, Mitsuji Saitou, Reiko Fujii, Naoko Moriwaki, Tokihiko Ogawa |
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Rok vydání: | 1992 |
Předmět: | |
Zdroj: | Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi). 33:237-240_1 |
ISSN: | 1882-1006 0015-6426 |
DOI: | 10.3358/shokueishi.33.237 |
Popis: | An analytical method of tetramine (tetramethylammonium, TM) in the salivary gland of gastropods with tetrabromophenolphthalein ethyl ester (TBPE) as an ion-pairing counter-ion was developed.TM was extracted into 1, 2-dichloroethane with TBPE under strongly alkaline conditions. Other quaternary ammonium species and amines tested did not interfere with the determination of TM. The ion-associate showed an absorption maximum at 610nm. Recovery of TM-Cl from the salivary gland was 100.2±2.3% and the determination limit was 0.20mg/g.Contents of TM-Cl in the salivary gland of gastropods were in the range of 2.39-6.08mg/g |
Databáze: | OpenAIRE |
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