Simultaneous cyclic-injection spectrophotometric determination of aluminum and iron in petroleum products

Autor:	A. Yu. Shishov, A. L. Moskvin, Leonid Moskvin, Andrey Bulatov
Rok vydání:	2014
Předmět:	Detection limit Analyte medicine.diagnostic_test business.industry Analytical chemistry chemistry.chemical_element Chrome azurol S Marine fuel Analytical Chemistry Chemometrics Petroleum product chemistry Aluminium Spectrophotometry medicine business Nuclear chemistry
Zdroj:	Journal of Analytical Chemistry. 69:1159-1164
ISSN:	1608-3199 1061-9348
Popis:	A procedure is developed for the cyclic-injection spectrophotometric determination of iron and aluminum in petroleum products; it includes microwave sample mineralization followed by the determination of analytes as their complexes with Chrome Azurol S at pH 5. The classical least-squares technique is used for the simultaneous determination of iron and aluminum. The analytical range for elements covers from 10 to 100 mg/kg at a sample weight of 1 g. The limits of detection for both elements are 3 mg/kg. The developed procedure was used for the determination of iron and aluminum in the spent engine oil and marine fuel.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::c82d4df12a32461d2b8d199231431c98 https://doi.org/10.1134/s1061934814120132 Zobrazit plný text záznamu Plný text ve formátu PDF