A ConvenientN-Protection of Pyroglutamate Derivatives
Autor: | Yasuo Kikugawa, Takeshi Sakamoto, Miyako Kato, Hao Li |
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Rok vydání: | 1995 |
Předmět: | |
Zdroj: | Synthetic Communications. 25:4045-4052 |
ISSN: | 1532-2432 0039-7911 |
DOI: | 10.1080/00397919508011481 |
Popis: | Esters of pyroglutamic acid were N-protected by conventional protective groups (Z. Boc, and COOMe) in high yield, without racemization, using LiHMDS in THF at - 78 °C and ZCl, Boc2O, and ClCOOMe, respectively. |
Databáze: | OpenAIRE |
Externí odkaz: |