Synthesis of Pure Lithium Amide Nanoparticles

Autor:	Neil M. Boag, Gael Baldissin, D. J. Bull, Chiu C. Tang
Rok vydání:	2013
Předmět:	Inorganic Chemistry chemistry.chemical_compound Hydrogen storage Deprotonation Lithium amide chemistry Transmission electron microscopy Inorganic chemistry Thermal decomposition chemistry.chemical_element Nanoparticle Lithium imide Lithium
Zdroj:	European Journal of Inorganic Chemistry. 2013:1993-1996
ISSN:	1099-0682 1434-1948
DOI:	10.1002/ejic.201201535
Popis:	Deprotonation of ammonia with n-butyllithium offers a facile synthetic route to produce pure lithium amide exhibiting fine granularity, which facilitates the complete thermal decomposition to lithium imide at a relatively low temperature of 600 K. Synthesised compounds were characterised by high-resolution synchrotron X-ray diffraction, and the particle morphology of lithium amide was studied by transmission electron microscopy. The proposed methodology readily affords the production of pure lithium amide nanoparticles at both bench-top and commercial scale.
Databáze:	OpenAIRE
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