Autor: |
Shan Shan Gong, Xiao Chuan Li, Qi Sun |
Rok vydání: |
2014 |
Předmět: |
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Zdroj: |
Applied Mechanics and Materials. 662:67-70 |
ISSN: |
1662-7482 |
DOI: |
10.4028/www.scientific.net/amm.662.67 |
Popis: |
A series of α-aminophosphonate-functionalized 3-aminopropanols have been efficiently prepared and characterized by1H,13C, and31P NMR and mass spectroscopy. The reaction conditions such as solvent and temperature were thoroughly investigated based on the three-component Kabachnik-Fields reaction. The experimental results revealed that moderate elevation of reaction temperature under solvent-free conditions was optimal for the synthesis of these types of compounds without forming the cyclized byproduct. |
Databáze: |
OpenAIRE |
Externí odkaz: |
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