Synthesis and characterization of zinc sulphide nanoparticles embedded in polymeric matrix
Autor: | A. Syed Mohamad, Chinnapiyan Vedhi, I. Merlin, G. Kavitha |
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Rok vydání: | 2022 |
Předmět: |
010302 applied physics
Materials science Scanning electron microscope technology industry and agriculture Nanoparticle macromolecular substances 02 engineering and technology 021001 nanoscience & nanotechnology 01 natural sciences chemistry.chemical_compound Aniline chemistry Chemical engineering Polymerization Transmission electron microscopy 0103 physical sciences Oxidizing agent Polyaniline Fourier transform infrared spectroscopy 0210 nano-technology |
Zdroj: | Materials Today: Proceedings. 48:196-200 |
ISSN: | 2214-7853 |
Popis: | Nano composites of conducting polyaniline with ZnS nanoparticles (PANI/ZnS) have been synthesized by in-situ polymerization of aniline monomer using ammonium persulphate as oxidizing agent. The formation of PANI/ZnS composites was assessed by UV–Vis spectroscopy, Transmission Electron Microscopy (TEM), Fourier Transform Infra-Red Spectroscope (FTIR), Atomic Force Microscope (AFM), Scanning Electron Microscope (SEM) and X ray diffraction analysis (XRD). FTIR and UV studies provided the information of functional group and optical behavior respectively SEM studies shows the well dispersion of ZnS Nanoparticles in the polyaniline matrix. Size determination identified and confirmed by TEM analysis. |
Databáze: | OpenAIRE |
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