Effect of Thermal Treatment on the Photocatalytic Activity in Visible Light of TiO2-W Flame Spray Synthesised Nanopowders
| Autor: | Katarzyna A. Michalow, Mieczyslaw Rekas, Kazimierz Kowalski, Martin Amberg, Andri Vital, Giuseppino Fortunato, Andre Heel, Thomas Graule |
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| Rok vydání: | 2009 |
| Předmět: |
Thermogravimetric analysis
Materials science technology industry and agriculture Analytical chemistry General Chemistry Thermal treatment Catalysis Differential scanning calorimetry X-ray photoelectron spectroscopy Transmission electron microscopy Photocatalysis Thermal spraying Nuclear chemistry Visible spectrum |
| Zdroj: | Topics in Catalysis. 52:1051-1059 |
| ISSN: | 1572-9028 1022-5528 |
| DOI: | 10.1007/s11244-009-9256-7 |
| Popis: | Effect of W doping as well as a thermal treatment on the structural and photocatalytic properties of TiO2 produced by flame spray synthesis (FSS) were the subject of investigation. Structural properties were studied by means of X-ray diffraction (XRD), BET adsorption isotherm and transmission electron microscopy (TEM). The surface condition was investigated by X-ray photoelectron spectroscopy (XPS) and differential scanning calorimetry (DSC) and differential thermal and thermogravimetric analysis (DTA-TGA). The photocatalytic properties were studied by optical measurements and photodecomposition of methylene blue under visible irradiation. It was found that the photoactivity in the visible region was enhanced significantly by the W-doping as well as by additional thermal treatment of those nanopowders. The obtained TiO2-W nanopowders exhibited higher performance under visible light than P25. |
| Databáze: | OpenAIRE |
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