Effect of Pineapple Leaf Fibers (PALF) concentration on nanofibers formation by electrospinning
Autor: | Khairunnadim Ahmad Sekak, Noor Najmi Bonnia, Siti Norasmah Surip, F. M. Abdul Aziz |
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Rok vydání: | 2018 |
Předmět: |
Materials science
02 engineering and technology 010402 general chemistry 021001 nanoscience & nanotechnology 01 natural sciences Electrospinning 0104 chemical sciences Solvent chemistry.chemical_compound Membrane chemistry Chemical engineering Nanofiber Lignin Hemicellulose Cellulose Fourier transform infrared spectroscopy 0210 nano-technology |
Zdroj: | IOP Conference Series: Materials Science and Engineering. 290:012003 |
ISSN: | 1757-899X 1757-8981 |
DOI: | 10.1088/1757-899x/290/1/012003 |
Popis: | Electrospinning method has been studied widely in producing nanofibers due to its straightforward and versatile method. In this study, Pineapple Leaf Fibers (PALF) solution were electrospinning to obtain mat of PALF electrospun. PALF were diluted in Trifluoacetic Acid (TFA) into five different concentrations to study the effect of concentration to the nanofibers formation. Raw sample of PALF (PALFraw), PALF after dewax (PALFdewax) and PALF after dilute with TFA (PALFTFA) were analyzed and compared using FTIR to study the structural change occur. TFA solvent has removed and recreated some of the functional group in PALF thus disrupt strong hydrogen bonds that hold hemicellulose, cellulose and lignin together. All the PALF sample has been proceed to electrospinning process. Low concentration of solution cause the solution jet to break up even before reach the collector however high concentration of solution made the solvent volatile faster and the solution dried easily. Therefore, PALF with optimum concentration of 0.02 gml-1 had favors the formation of nanofibers and succeed in forming membrane at the collector. |
Databáze: | OpenAIRE |
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