The synthesis of mono-dispersed ε-Fe3N nanoparticles by gas phase reaction with controlled annealing conditions
| Autor: | Fanguo Li, Shoufa Liu |
|---|---|
| Rok vydání: | 2018 |
| Předmět: |
010302 applied physics
Materials science Annealing (metallurgy) Mechanical Engineering Nanoparticle 02 engineering and technology Crystal structure 021001 nanoscience & nanotechnology Condensed Matter Physics 01 natural sciences law.invention Iron pentacarbonyl Magnetization chemistry.chemical_compound Ammonia Chemical engineering chemistry Mechanics of Materials law Lattice (order) 0103 physical sciences General Materials Science Crystallization 0210 nano-technology |
| Zdroj: | Materials Letters. 221:161-164 |
| ISSN: | 0167-577X |
| Popis: | This paper reported a gas phase reaction to synthesize e-Fe 3 N nanoparticles with controlled annealing conditions. Vaporized iron pentacarbonyl (Fe(CO) 5 ) was used as the iron source, and ammonia (NH 3 ) was used as the nitrogen source. In three parallel experiments, the annealing time of the nanoparticles was controlled. The particle morphologies and lattice parameters of the as-synthesized particles were characterized by TEM, and the crystal structure and crystallization level were determined by XRD. The magnetic properties were measured by VSM. The experimental results showed that enhanced crystallization and magnetization were obtained on the nanoparticles with longer annealing time. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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