Preparation and Characterization of Silicone Oil/UF Resin Microcapsules as Erosion Inhibitor
Autor: | Shao Sen Lin, De Jiang Lin, Shi Guo Du, Hong Guang Li |
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Rok vydání: | 2016 |
Předmět: |
Materials science
Silicon dioxide Scanning electron microscope 020209 energy Mechanical Engineering Infrared spectroscopy 02 engineering and technology Silicone oil chemistry.chemical_compound chemistry Polymerization Chemical engineering Mechanics of Materials 0202 electrical engineering electronic engineering information engineering General Materials Science Particle size Composite material In situ polymerization Pyrolysis |
Zdroj: | Key Engineering Materials. 723:481-485 |
ISSN: | 1662-9795 |
DOI: | 10.4028/www.scientific.net/kem.723.481 |
Popis: | Microcapsules with silicone oil as core and poly (urea-formaldehyde) as shell were prepared by direct in-situ polymerization process. The influences of formaldehyde-urea molar ratios on microcapsules morphologies were investigated by scanning electron microscope (SEM). The microcapsules were characterized by fourier transform infrared spectrometer (FT-IR), particle size analyzer, simultaneous thermal analyzer. The results showed that well dispersive microcapsules were obtained with average particle size of 2.5 μm when formaldehyde-urea molar ratio was 1.8:1.0 and that the weight ratio of silicon dioxide to microcapsule was 15.4%, which produced from pyrolysis of core material silicone oil. The prepared microcapsules were expected to a kind of high-efficiency erosion inhibitor when used in propellant. |
Databáze: | OpenAIRE |
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