Synthesis of bicyclic systems containing fused sulfolane and isoxazolidine rings

Autor:	A. V. Serebryannikova, V. M. Berestovitskaya, L. V. Lapshina, Vladislav V. Gurzhiy, I. E. Efremova
Rok vydání:	2018
Předmět:	Bicyclic molecule 010405 organic chemistry Organic Chemistry Infrared spectroscopy Nuclear magnetic resonance spectroscopy 010402 general chemistry 01 natural sciences 0104 chemical sciences chemistry.chemical_compound Hydroxylamine chemistry Organic chemistry Sulfolane Isoxazole
Zdroj:	Chemistry of Heterocyclic Compounds. 54:76-82
ISSN:	1573-8353 0009-3122
Popis:	A method was developed based on reactions of 2-benzylidene-3-methyl-4-nitro-3-thiolene 1,1-dioxide and its substituted analogs with hydroxylamine and N-methylhydroxylamine for the synthesis of 3-aryl-6а-methyl-6-nitrohexahydrothieno[2,3-d]isoxazole 4,4-dioxides – new representatives of original bicyclic structures combining condensed isoxazolidine and sulfolane rings. The structures of the obtained compounds were established by methods of IR spectroscopy, one-dimensional 1Н and 13С NMR spectroscopy, two-dimensional 1Н–13С HMQC and 1Н–13С HMBC experiments, and X-ray structural analysis.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::4506bff22ddd3999913d596792fc3e4d https://doi.org/10.1007/s10593-018-2233-y Zobrazit plný text záznamu Plný text ve formátu PDF Plný text ve formátu HTML
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