Macrosegregation During Re-melting and Holding of Directionally Solidified Al-7 wt.% Si Alloy in Microgravity
Autor: | M. Lauer, R. N. Grugel, Samuel Angart, D. R. Poirier, M. Ghods, S. N. Tewari |
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Rok vydání: | 2017 |
Předmět: |
010302 applied physics
Materials science Buoyancy Silicon Metallurgy Alloy General Engineering chemistry.chemical_element 02 engineering and technology Electron microprobe engineering.material 021001 nanoscience & nanotechnology 01 natural sciences Rod Temperature gradient chemistry 0103 physical sciences engineering General Materials Science 0210 nano-technology Directional solidification Eutectic system |
Zdroj: | JOM. 69:1289-1297 |
ISSN: | 1543-1851 1047-4838 |
DOI: | 10.1007/s11837-017-2380-0 |
Popis: | As-cast aluminum-7 wt.% ailicon alloy sample rods were re-melted and directionally solidified on Earth which resulted in uniform dendritically aligned arrays. These arrays were then partially back-melted through an imposed, and constant, temperature gradient in the microgravity environment aboard the International Space Station. The mushy zones that developed in the seed crystals were held for different periods prior to initiating directional solidification. Upon return, examination of the initial mushy-zone regions exhibited significant macrosegregation in terms of a solute-depleted zone that increased as a function of the holding time. The silicon (solute) content in these regions was measured on prepared longitudinal sections by electron microprobe analysis as well as by determining the fraction eutectic on several transverse sections. The silicon content was found to increase up the temperature gradient resulting in significant silicon concentration immediately ahead of the mushy-zone tips. The measured macrosegregation agrees well with calculations from a mathematical model developed to simulate the re-melting and holding process. The results, due to processing in a microgravity environment where buoyancy and thermosolutal convection are minimized, serve as benchmark solidification data. |
Databáze: | OpenAIRE |
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