Development of an analytical method for cholesterol determination in feed for ruminants using factorial experimental design

Autor:	Bandeira, Cecilia Muller, Ferreira, Jose Maria, Bragagnolo, Neura, Lilian Mariutti
Předmět:	GC validation extraction
Zdroj:	ResearcherID Química Nova, Volume: 31, Issue: 6, Pages: 1422-1426, Published: 2008
Popis:	A chromatographic method was developed for cholesterol determination in feed for ruminants using response surface methodology. Among the five approaches of sample preparation methods tested, the saponification of the sample without heating presented less interference in the gas chromatography. The method presented a relative standard deviation (RSD) of 4.3%, recoveries between 84 and 87% and detection limit of 0.001 mg of cholesterol per g of feed.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=dedup_wf_001::d7cf589b54f77a0f6403706ee70028b6 http://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=ORCID&SrcApp=OrcidOrg&DestLinkType=FullRecord&DestApp=WOS_CPL&KeyUT=WOS:000259796500027&KeyUID=WOS:000259796500027 Zobrazit plný text záznamu