14C GIRI SAMPLES IN AMS GOLDEN VALLEY: GRAPHITE PREPARATION USING AGE-3 AND ABSORPTION-CATALYTIC SETUP

Autor: Parkhomchuk, E V, Petrozhitskiy, A V, Ignatov, M M, Kuleshov, D V, Lysikov, A I, Okunev, A G, Babina, K A, Parkhomchuk, V V, Boaretto, Elisabetta, Hajdas, Irka, Synal, Hans-Arno
Zdroj: Radiocarbon; October 2024, Vol. 66 Issue: 5 p1259-1269, 11p
Abstrakt: ABSTRACTThe AMS Golden Valley laboratory is equipped with two accelerator mass spectrometers: the AMS facility from the Budker Institute of Nuclear Physics (BINP) and the Mini Carbon Dating System (MICADAS-28) from Ionplus AG and two graphitization systems: the Automated Graphitization Equipment (AGE-3) from Ionplus AG and the Absorption-catalytic setup (ACS) developed at the Boreskov Institute of Catalysis (BIC). The ACS was designed for graphite preparation from labeled biomedical samples, dissolved organics, and dissolved or gaseous carbon dioxide but has proven to be suitable for the traditional dating of objects no older than 35,000 years. Here we present two series of AMS data for the samples from Glasgow International Radiocarbon Inter-comparison (GIRI), prepared using AGE-3 and ACS, and then measured on MICADAS-28. The mean value of the background F14C was 0.0024 ± 0.0009 and 0.012 ± 0.003 for AGE-3 and ACS, respectively, and both methods gave reproducible results for the OXI.
Databáze: Supplemental Index