How acid attack and high temperature affect the microstructure of adsorbent geopolymers

Autor: Tochetto, Gabriel André, Simão, Lisandro, Pavan Korf, Eduardo, de Oliveira, Débora, Hotza, Dachamir, Serafini Immich, Ana Paula
Zdroj: Open Ceramics; 20230101, Issue: Preprints
Abstrakt: Geopolymers (GPs) are versatile materials that have low intrinsic porosity. This characteristic can be used as a motivator for the development of porous GPs, since separation processes require adsorbents with a high specific area. Thus, this work aimed to elucidate how acid attack and calcination affect the microstructure of GPs. For this purpose, a GP was exposed to H2SO4and 200 °C, being later characterized in terms of morphology, mineralogy, functional groups, and textural properties. Acid etching and calcination proved to be effective strategies for surface area improvement, making the modified GP a strong candidate for use as an adsorbent.
Databáze: Supplemental Index