| Abstrakt: |
Abstract: A fairly simple radiometric method has been developed for the quantitation of microgram amounts of mercury in lead samples of different purity grades. It is mainly based on 3 steps; (i) the removal of most interfering cations with ferric hydroxide scavenger in the presence of a suitable masking agent, (ii) the separation of mercury as hydrated mercuric oxide from a highly alkaline medium, (iii) its distillation as mercuric chloride followed by precipitation as the sulfide. The method is reproducible and the results which show, in general, a standard deviation of ±4.29% are compared with those obtained by atomic absorption (4.48%) and spectrophotometric (13.13%) techniques. |
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