The crystal structure of Chrysosplenol D, C18H16O8.

Autor: Li, Yijv, Zhao, Nengwu, Ye, Jianghai, Xu, Fangfang, Luo, Shuntong, Lang, Tianqiong
Předmět:
Zdroj: Zeitschrift für Kristallographie / New Crystal Structures; Oct2022, Vol. 237 Issue 5, p877-879, 3p
Abstrakt: Detailed analysis of its crystal structure revealed that the methoxyl groups located at C-3 and C-6 are turned out from the plane of chromone skeleton, which is in accordance with that of casticin, the methyl etherified derivative at 4'-OH of the title compound [[11], [13]]. The title compound (131.8 mg) was obtained from the E4 fraction I via i repeated silica gel column chromatography. The ethyl acetate fraction (0.219 kg) was then separated over silica gel column chromatography eluted with petroleum ether/ethyl acetate and dichloromethane/methanol in gradient, affording six fractions of E1-E6. [Extracted from the article]
Databáze: Complementary Index