Reaction of Sodium 4-Acetyl-1-phenyl-1H-1,2,3-triazol-5-olate with 1,2,3-Thiadiazole-4-carboxylic Acid Hydrazide.

Autor: Tokareva, M. A., Obydennov, K. L., Slepukhin, P. A., Vysokova, O. A., Glukhareva, T. V.
Předmět:
Zdroj: AIP Conference Proceedings; 2019, Vol. 2063 Issue 1, p040060-1-040060-5, 5p, 5 Diagrams, 1 Graph
Abstrakt: The present work describes a method for the synthesis a new N-1,2,3-triazol-1-yl-1,2,3-thiadiazol-4-carboxamide via condensation of open-chain form of 4-acetyl-1,2,3-triazolium-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide, followed by formation new 1,2,3-triazole cycle. The structure of synthesized compound was characterized by spectroscopic methods such as ¹H NMR, 13C NMR, IR, mass spectrometry and X-ray diffraction. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index