Effect of hydrofluoric acid concentration and aging on the bond strength ceramics to a resin cement.

Autor: Clerot BD; Department of Orthodontics, Graduate Program in Orthodontics - UNIARARAS, Universidade de Araras, SP, Brazil., Correr-Sobrinho L; Department of Restorative Dentistry, Dental Materials Division, Piracicaba Dental School, UNICAMP, State University of Campinas, Piracicaba, SP, Brazil., Bandini M; Department of Orthodontics, Graduate Program in Orthodontics - UNIARARAS, Universidade de Araras, SP, Brazil., Pinheiro Beserra-Neto E; Department of Restorative Dentistry, Dental Materials Division, Piracicaba Dental School, UNICAMP, State University of Campinas, Piracicaba, SP, Brazil., Tsuzuki FM; Department of Restorative Dentistry, Dental Materials Division, Piracicaba Dental School, UNICAMP, State University of Campinas, Piracicaba, SP, Brazil., Pacheco RR; Department of Restorative Sciences, The Dental College of Georgia at Augusta University, Augusta, GA, USA., Costa AR; Department of Orthodontics, Graduate Program in Orthodontics - UNIARARAS, Universidade de Araras, SP, Brazil.
Jazyk: angličtina
Zdroj: Brazilian dental journal [Braz Dent J] 2024 Jul 22; Vol. 35, pp. 5669. Date of Electronic Publication: 2024 Jul 22 (Print Publication: 2024).
DOI: 10.1590/0103-6440202405669
Abstrakt: This study evaluated the influence of hydrofluoric acid (HF) concentration and thermal cycling on the microshear bond strength (µSBS) of a resin luting agent to IPS e.max® CAD and Rosetta® SM. Ceramic specimens (12.0 x 14.0 x 1.5mm) were randomized into 8 groups (n=10) according to HF concentration, commercial brand, and aging. Immediately after polishing, and etching, all specimens were silanized and a layer of adhesive was applied. A PVS mold of 3 mm thickness and 10mm diameter with (four) 1.0mm holes was fabricated, placed on each specimen, and then filled with a resin luting agent. Half of the specimens were subjected to the µSBS test using an Instron at a speed of 1.0 mm/min, following a 24-hour storage in deionized water at 37ºC. The remaining specimens were subjected to thermal cycling (5ºC-55ºC, 30 seconds per bath) and µSBS. The data were evaluated utilizing a three-way ANOVA and Tukey's post-hoc test (α=0.05). Significant differences were found for HF concentration and aging (p<0.0001). No significant difference in µSBS was found for commercial brands (p=0.085). The interaction between brand and HF concentration (p=0.358), brand and aging (p=0.135), and HF concentration and aging (p=0.138) were not statistically significant. The triple interaction among these factors was not statistically significant (p=0.610). In conclusion, the bond strength is affected by the HF concentration. No statistical difference was observed between the two ceramics. Thermal cycling significantly reduced µSBS.
Databáze: MEDLINE