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pro vyhledávání: '"and Bradley A. Sleadd"'
Publikováno v:
Organometallics. 20:4956-4964
High-yield syntheses of the novel cations cis-Ru(N−N)(η2-tpy)(CO)22+2PF6- (2a,b: N−N = 2,2‘-bipyridine, tpy = 2,2‘:6‘,2‘ ‘-terpyridine; 5a,b: N−N = 4,4‘-dimethyl-2,2‘-bipyridine) have been develo...
Autor:
Mark S. Mashuta, Judith C. Gallucci, and Bradley A. Sleadd, Brian Niemann, Bhamidi Srinivas, Dorothy H. Gibson, Ashwani Vij
Publikováno v:
Organometallics. 19:4179-4182
Reaction of cis-Ru(bpy)2(CO)CH2OH+PF6- (1, bpy = 2,2‘-bipyridine) with acetic anhydride yields the corresponding acetoxymethyl derivative 2. However, reaction of 1 with a large excess of acetic acid in acetonitrile yields compound 3, containing an
Autor:
Bradley A. Sleadd, Yan Ding, Dorothy H. Gibson, Mark S. Mashuta, Rebecca L Miller, John F. Richardson
Publikováno v:
Polyhedron. 18:1189-1200
New formate ( 1 – 3 ; 4b , 6 and 7 ), acetate ( 8 , 9) and trifluoroacetate ( 12 , 13 and 15 ) complexes have been synthesized and characterized by elemental analysis and by IR and 1 H and 13 C NMR spectroscopies. New data or new synthetic procedur
Publikováno v:
Journal of Chemical Crystallography. 29:619-622
The title compound, fac-(2,2′-bipyridyl)(carbomethoxy)rhenium tricarbonyl, crystallizes in the monoclinic system, space group P21/c with the following crystal data: a = 8.37551(1), b = 6.6934(1), c = 26.2098(1) A, V(A3) = 1535.93(3), Z = 4, and β
Publikováno v:
Organometallics. 16:4421-4427
Reaction of cis-Ru(tpy)(CO)2Cl+PF6- (1; tpy = 2,2‘:6‘,2‘‘-terpyridyl) with aqueous Na2CO3 in acetonitrile yields the CO2-bridged complex cis,cis-(CH3CN)(CO)(tpy)Ru(CO2)Ru(tpy)(CO)22+2PF6- (3). Reaction of 1 with aqueous NaOCHO yields the corr
Publikováno v:
Organometallics. 14:4886-4891
Autor:
Win Naing, Mark S. Mashuta, Dorothy H. Gibson, Jaime O. Franco, Bradley A. Sleadd, John F. Richardson
Publikováno v:
Organometallics. 13:4570-4577
Publikováno v:
Organometallics. 17:2689-2691
Photoassisted reactions of fac-Re(bpy)(CO)3(CH2OR) (1, R = H; 2, R = OAc) and fac-Re(bpy)(CO)3CH2Ph (5) in MeOH provide fac-Re(bpy)(CO)3(OCH3) (3); 2 and 3 have been structurally characterized. Radical paths are indicated for 2 and 5; a nonradical pa
Autor:
Jaime O. Franco, Bradley A. Sleadd, Dorothy H. Gibson, Yan Ding, John F. Richardson, Mark S. Mashuta
Publikováno v:
Journal of the American Chemical Society. 118:11984-11985
Prior to the recent report of the synthesis of cis-Ru(bpy){sub 2} (CO)(CHO){sup +}PF{sub 6}{sup -} (1; bpy = 2,2`-bipyridyl) by Tanaka et al., we had also synthesized the compound and begun a study of its reactions. We now describe our observations o