Zobrazeno 1 - 10
of 38
pro vyhledávání: '"Zbigniew Marcinow"'
Publikováno v:
Tetrahedron. 57:3637-3644
New, non-pyrolytic methods are presented for the synthesis of curved-surface, polynuclear aromatic hydrocarbons related to the fullerenes. Tetrabromocorannulene is conveniently prepared on a large scale and then converted to corannulene, and also use
Publikováno v:
Tetrahedron Letters. 41:9931-9934
Synthesis of a number of substituted corannulenes and dibenzo[a,g]corannulenes starting from 1,2,5,6-tetrabromocorannulene 3 is described. Since 3 is conveniently obtained by a large scale, non-pyrolytic route, it may serve as a synthon for the furth
Publikováno v:
Tetrahedron Letters. 39:9127-9130
1,2-Diarylethanes and 1,2-diarylethylenes can be oxidized directly to 1,2-diaryldiketones in good yields by reaction with benzeneseleninic anyhdride (BSA) at 120 °C in chlorobenzene.
Autor:
Renata Sygula, Atteye H. Abdourazak, Zbigniew Marcinow, Haskell E. Folsom, Peter W. Rabideau, Frank R. Fronczek, Andrzej Sygula
Publikováno v:
Tetrahedron Letters. 35:3857-3860
The title compound is conveniently synthesized from the known 1,2-diketopyracene via NBS bromination followed by reaction with silver nitrate in acetonitrile, and treatment with sodium acetate trihydrate in DMSO. Its structure determined by semiempir
Publikováno v:
The Journal of Organic Chemistry. 67:3537-3539
The flash vacuum pyrolysis (FVP) of 1,2-bis(2-bromophenyl)-4,9-dibromocorannulene leads to a new C(32)H(12) buckybowl.
Publikováno v:
Tetrahedron Letters. 34:6351-6354
The question of an anion within an anion structure for corannulane tetraanion is examined by ab initio and semi-empirical calculations, as well as by the behavior of corannulene anionic intermediates in anhydrous ammonia. Calculations do not lend muc
Publikováno v:
ChemInform. 28
The authors have provided an improved synthesis of 1,2,5,6-tetraketopyracene (6), in that three steps have been replaced with one high-yield step. Moreover, a very unreliable step has been eliminated. In turn, this has led to an improved synthesis of
Autor:
Peter W. Rabideau, Zbigniew Marcinow
Publikováno v:
ChemInform. 24
The reduction of aromatic compounds by alkali metals in liquid ammonia represents an important method for the preparation of partially unsaturated six-membered rings. The reaction was discovered by Wooster and Godfrey, but the major development resul
Publikováno v:
ChemInform. 26
Publikováno v:
ChemInform. 27