Zobrazeno 1 - 10
of 22
pro vyhledávání: '"W. E. Lynch"'
Publikováno v:
Acta Crystallographica Section E: Crystallographic Communications
Acta Crystallographica Section E: Crystallographic Communications, Vol 75, Iss 8, Pp 1284-1290 (2019)
Acta Crystallographica Section E: Crystallographic Communications, Vol 75, Iss 8, Pp 1284-1290 (2019)
The synthesis and crystal structures of four dimeric complexes composed of manganese(II) dibromide, a pyridine N-oxide and solvent molecules are reported. The pyridine N--oxide, 2-methylpyridine N-oxide, 3-methylpyridine N-oxide, and 4-methyl
Autor:
Nathan Peek, Brandon Quillian, W. E. Lynch, Delana Nivens, John W. Stone, Clifford W. Padgett, Anthony Petrillo
Publikováno v:
Journal of Molecular Structure. 1185:99-106
Reaction of tetrakis(acetonitrile)copper(I) perchlorate ([Cu(NCCH3)4][ClO4]), tris-1-ethyl-4-methylimidazolylphosphine (T1Et4MeIP) (1) and 3-hydroxyflavone (flavH) under ambient conditions produces an in-situ generated flavonol bound copper(II) compl
Publikováno v:
IUCrData, Vol 5, Iss 10, p x201335 (2020)
Our work in the area of synthesis of metal–organic frameworks (MOFs) based on organic N-oxides led to the crystallization of pyridine-4-carboxamidoxime N-oxide. Herein we report the first crystal structure of the title compound, C6H7N3O2 [systemati
Publikováno v:
IUCrData, Vol 5, Iss 9, p x201205 (2020)
Our work in the area of synthesis of tris indole compounds as a potential chelator led to the synthesis and crystallization of ethyl 1H-indole-2-carboxylate, C11H11NO2, an indole that was synthesized by the thionyl chloride reaction of 1H-indole-2-ca
Publikováno v:
Acta Crystallographica Section E: Crystallographic Communications, Vol 74, Iss 10, Pp 1405-1410 (2018)
Manganese(II) acetate coordination polymers have been prepared with three derivatives of pyridine N-oxide. The compounds are catena-poly[manganese(II)-μ3-acetato-di-μ2-acetato-[aquamanganese(II)]-μ2-acetato-μ-(pyridine N-oxide)-manganese(II)-μ3-
Autor:
Michael Tran, Brandon Quillian, Anthony Petrillo, Alexis Lorbecki, W. E. Lynch, Clifford W. Padgett
Publikováno v:
Journal of Chemical Crystallography. 49:1-7
The reaction of bis(pyrazol-1-yl)acetic acid (L) with copper(II) bromide provides two new complexes: [Cu(L-H)Br(µ-Br)]2 (1) and [Cu(L)2]⋅4H2O (2). Complex 1 is prepared by the stoichiometric reaction of L-H with copper(II) bromide in tetrahydrofur
Autor:
Joseph R. Traver, Patrick C. Hillesheim, Gary L. Guillet, W. E. Lynch, Erica Chenard, Matthias Zeller
Publikováno v:
Journal of Molecular Structure. 1232:130046
A series of ionic compounds based on the dicationic vitamin B1 structure have been synthesized and characterized. A set of perfluoroalkyl-based anions, each with a distinct structure, were paired with the cations and the solid-state structures of the
Autor:
Joseph G. Bazemore, W. E. Lynch, Anthony Petrillo, Clifford W. Padgett, Elizabeth M. Beasley, Brandon Quillian
Publikováno v:
Inorganica Chimica Acta. 512:119855
The reaction of 3-hydroxyflavone with copper(II) bromide in various alcohols (ethanol, isopropanol, and methanol) yielded a mixture of their respective 3-hydroxy-2,3-dialkoxy-2-phenylchroman-4-ones (hemiacetals) and 3,3-dihydroxy-2-alkoxy-2-phenylchr
Publikováno v:
IUCrData, Vol 3, Iss 8, p x181138 (2018)
Our work in the area of carbon-monoxide-releasing molecules led to the synthesis and crystallization of new flavone derivatives as intermediates. Herein we report the first crystal structure of the title compound, C16H12O3, a hydroxy-substituted flav
Autor:
W. E. Lynch, Clifford W. Padgett
Publikováno v:
IUCrData, Vol 3, Iss 3, p x180320 (2018)
In the title co-crystal, C10H8N2O2S2·H2O2, both molecules are generated by crystallographic twofold symmetry; the dihedral angle between the pyridine rings is 101.16 (9)°. In the crystal, the components are linked by O—H...O hydrogen bonds to gen