Zobrazeno 1 - 10
of 21
pro vyhledávání: '"V. L. Varand"'
Publikováno v:
Journal of Analytical Chemistry. 64:843-846
A procedure is developed for the coulometric determination of amine-substituted derivatives of 1,2,4-triazole. Stoichiometric coefficients of 1,2,4-triazoles and transition metal complexes with these ligands in bromination reactions are determined. T
Publikováno v:
Russian Journal of Coordination Chemistry. 34:931-937
The heteroligand complex Nd(Phen){(iso-C4H9)2PS2}2(NO3) (I) was synthesized and its IR spectrum was analyzed. The anions (iso-C4H9)2PS2/− and N3/− act as bidentate cyclic ligands. The single crystals of [Nd(Phen){iso-C4H9)2PS2}3] (II) were obtain
Publikováno v:
Journal of Structural Chemistry. 49:175-180
The [Y(Phen){(i-C4H9)2PS2}2NO3] mixed-ligand compound (I) was synthesized. Its structure was determined by X-ray diffraction analysis (X8 APEX diffractometer, λMoK α , 3788 F hkl , R = 0.0677). Crystals I are orthorhombic: a = 10.6495(8) A, b = 20.
Autor:
A. A. Lobanova, V. L. Varand, N. I. Popov, S. V. Larionov, I. V. Kazantsev, Sergey G. Il'yasov
Publikováno v:
Russian Journal of General Chemistry. 76:1719-1723
Chelates M(O2NNCONHNH2)2 · 2H2O (M = Fe, Co, Ni, Zn) were prepared by the reactions of 4-nitrosemicarbazide with appropriate 3d transition metal salts. The structures of the compounds were suggested on the basis of data obtained by physicochemical m
Autor:
S. V. Trubina, I. M. Oglezneva, S. V. Larionov, N. A. Kryuchkova, T. E. Kokina, L. N. Mazalov, V. L. Varand, O. V. Tarasenko
Publikováno v:
Journal of Structural Chemistry. 46:542-545
X-ray photoelectron and voltammetry studies of the charged state of the metal atom in nickel(II) chelate complexes with ligands containing CS 2 − and PS 2 − groups and in heteroligand complexes on their basis were carried out. It is shown that th
Autor:
Liliya A. Sheludyakova, Galina V. Romanenko, N. P. Sokolova, V. P. Fadeeva, V. L. Varand, V. I. Lisoivan
Publikováno v:
Russian Journal of Coordination Chemistry. 29:362-368
Two isomers with empirical formula C6H6F9O9Tb are synthesized and their structures are studied. Isomerism was found to arise due to different positions of a proton. Crystals of two isomers are isostructural and form continuous series of solid solutio
Publikováno v:
Russian Journal of General Chemistry. 71:15-18
The system Eu(CF3CO2)3-Gd(CF3CO2)3-H2O, which forms solid solutions EuxGd1-x(CF3CO2)3 · 3H2O, was studied. The thermolysis of these solutions at 350-360°C yields solid solutions of lanthanide trifluorides. X-ray examination showed that these solid
Autor:
S. V. Larionov, Nina V. Podberezskaya, Galina V. Romanenko, D. Yu. Naumov, V. L. Varand, S. A. Gromilov
Publikováno v:
Journal of Structural Chemistry. 42:1036-1039
Publikováno v:
Journal of Structural Chemistry. 41:544-549
Autor:
L. G. Lavrenova, S. V. Larionov, Liliya A. Sheludyakova, V. A. Varnek, Vladimir N. Ikorskii, V. L. Varand, O. G. Shakirova, Yu. G. Shvedenkov, T. A. Krieger
Publikováno v:
Journal of Structural Chemistry. 41:790-797
The reaction of Fe(NO3)2, trz, and atrz in ethanol–water gave solid Fe(trz)3x(atrz)3-3x(NO3)2·H2O(x = 0.1, 0.2, 0.4, 0.8). The solids were investigated by magnetic chemistry, X-ray diffraction, photoelectron (DRS), IR, and Mossbauer spectroscopy m