Zobrazeno 1 - 10
of 20
pro vyhledávání: '"UTTAM KUMAR RAY"'
Autor:
Appalacharyulu Salapaka, Kishore Babu Bonige, Hemant Kumar Sharma, Uttam Kumar Ray, Raghu Babu Korupolu
Publikováno v:
Asian Pacific Journal of Health Sciences. 9:91-95
A simple and sensitive method based on capillary electrophoresis with UV detection was developed, optimized, and validated for the determination of five membered heterocyclic polar compound, imidazole in pharmaceutical drug substances. Separation was
Autor:
Uttam Kumar Ray, Annapurna Nowduri, Raghu Babu Korupolu, Sreenivasulu Boju, Sarvesh Kumar, Dhanraj T. S. S. Sundaram, Chandra Sekhara Rao Nethinti
Publikováno v:
Asian Journal of Chemical Sciences. :46-53
Pd-Catalyzed hydrogenation process has been developed to synthesize tetrahydrocurcumin from synthetic curcumin. Use of diphenyl sulphide as catalyst poison is crucial for lowering the activity of the catalyst and thus reduces impurity formation. The
Autor:
Appalacharyulu Salapaka, Kishore Babu Bonige, K. Chandrasekhar Reddy, Hemant Kumar Sharma, Uttam Kumar Ray
Publikováno v:
Asian Journal of Chemistry. 34:2587-2592
A simple, sensitive, selective and reproducible stability indicating reverse phase HPLC method has been developed and validated for the determination of related substances of linagliptin drug substance. Separation of impurities was carried out on a Y
Publikováno v:
Journal of Advanced Scientific Research. 12:198-209
Schiff base macrocycles play a significant role in living organisms with a broad range of pharmaceutical activities. In the present study, a novel series of 26 member macrocyclic compounds were synthesized via recombination of novel diamine and terep
Autor:
N. Sreenivas, Chandrasekhar Reddy T, Uttam Kumar Ray, Raghu Babu Korupolu, Hemant Sharma, Kishore Babu Bonige, Appalacharyulu Salapaka, Chandrasekhar Reddy K
Publikováno v:
ELECTROPHORESIS. 40:1066-1073
A simple, sensitive, and stability indicating isocratic reverse phase high performance liquid chromatography method has been developed, optimized and validated for the separation and quantification of S-enantiomer in linagliptin (R-enantiomer) drug s
Autor:
V. Kumar, N. Sreenivas, Vinay Kumar Patcha, K. S. R. Pavan Kumar, Susheela Bhai Gajbhiye, Uttam Kumar Ray
Publikováno v:
American Journal of PharmTech Research. 8:186-195
Publikováno v:
Medicinal Chemistry Research. 22:1624-1629
Microwave-assisted rapid and efficient procedure for the synthesis of bisphosphonate and their libraries is described in solvent-free medium. Bisphosphonates having nitrogen and sulfur are synthesized following this new procedure. This procedure is s
Autor:
Uttam Kumar Ray, G. Srikanth, D. V. N. Srinivas Rao, P. Lavanya, P. Badarinadh Gupta, Aminul Islam
Publikováno v:
Synthetic Communications. 42:1359-1366
A new and efficient process through a new intermediate, (2E)-2-cyano-3-(3,4-dihydroxy-5-nirtrophenyl)prop-2-enoic acid 15, has been described for preparing substantially pure entacapone 1. This new intermediate 15 was prepared by Knoevenagel condensa
Autor:
Hemant Sharma, Uttam Kumar Ray, Ch. Srinivas, K. Mukkanti, T. Joseph Sunder Raj, N. Rashmitha, N. Srinivas
Publikováno v:
E-Journal of Chemistry, Vol 7, Iss 2, Pp 555-563 (2010)
The present paper describes the development of a reverse phase chromatographic (RPLC) method for montelukast sodium in the presence of its impurities and degradation products generated from forced degradation studies. The drug substance was subjected
Autor:
Aminul Islam, N. Murali, V. Kumar, Srikanth Guntupalli, D. Satheesh, Uttam Kumar Ray, P. Badrinadh Gupta
Publikováno v:
Journal of pharmaceutical and biomedical analysis. 88
During the synthesis of ezetimibe, two process related impurities were detected were HPLC analysis at levels ranging from 0.05 to 0.8%. These two impurities were isolated by column chromatography and co-injected with ezetimibe sample to confirm the r