Zobrazeno 1 - 10
of 59
pro vyhledávání: '"Tomoya Machinami"'
Autor:
Takashi Fujimoto, Hiyori Furumachi, Yuta Morishita, Ayumi Tsutsui, Tomoya Machinami, Rina Hirai, Tomoyuki Fujita
Publikováno v:
Tetrahedron Letters. 68:152836
Glutathione (GSH) has two important biological activities, GSH conjugation and radical scavenging. In this work, we determined that GSH can participate in an intramolecular cyclization between the glutamic α-carboxylic acid and the cysteinyl thiol m
Autor:
Daisuke Miura, Tomoya Machinami
Publikováno v:
Modern Research in Catalysis. :20-27
Prolinamido-glycoside catalyzed asymmetric aldol reaction in aqueous media is reported. The reactions are rapid and highly stereoselective when water is used as solvent. The stereoselectivities were under influence of configurations of a prolyl resid
Publikováno v:
Synlett. 24:1501-1504
Prolinamido-glycosides, water-compatible organocatalysts, are capable of catalyzing the stereoselective aldol reaction in aqueous media. The aldol reaction of 2,2-dimethyl-1,3-dioxan-5-one with aldehydo sugars in the isopropylidene form gave ketoses
Autor:
Daisuke Miura, Mitsuru Tashiro, Takayuki Kato, Takashi Fujimoto, Tomoya Machinami, Osamu Kamo, Yuichi Shimoikeda
Publikováno v:
American Journal of Analytical Chemistry. :361-367
Complex formation of 1,6-anhydro-β-maltose and sodium ions was characterized using single-crystal X-ray crystallography and solution- and solid-state NMR spectroscopy. The 7-coordination structure, comprising two 1,6-anhydro-β-maltoses, a thiocyana
Autor:
Kenji Uéda, Sakurako Shimotakahara, Yoichi Shibusawa, Yuuki Shiroyama, Mitsuru Tashiro, Mai Akai, Sayaka Kado, Takaya Onoue, Takashi Fujimoto, Hiroko Seki, Tomoya Machinami
Publikováno v:
Journal of Biophysical Chemistry. :149-155
α-Synuclein is the major component of the filamentous Lewy bodies and Lewy neurites that define neuropathological features and dementia with Lewy bodies. To investigate the role of dopamine (DA) in α-synuclein fibrillation, the structural propensit
Autor:
Takashi Fujimoto, Takayuki Kato, Osamu Kamo, Tomoya Machinami, Kazuo Furihata, Toshiyo Kato, Mitsuru Tashiro, Yosuke Usui, Koji Tsubono
Publikováno v:
Carbohydrate Research. 346:1991-1996
The formation of a complex between 1,6-anhydro-β-maltose and potassium ions was characterized using (1)H, (13)C and (39)K NMR spectroscopy and single-crystal X-ray crystallography. In the NMR study, the spin-lattice relaxation times (T(1)) of C1, C3
Autor:
Kazuo Furihata, Koji Tsubono, Tomoya Machinami, Takayuki Kato, Mitsuru Tashiro, Takashi Fujimoto, Toshiyo Kato, Osamu Kamo
Publikováno v:
Magnetic Resonance in Chemistry. 47:948-952
The 1H and 39K longitudinal relaxation times (T1) and 1H diffusion coefficients were measured to investigate the complex formation of 1,6-anhydro-β-maltotriose and potassium ions. Although the 1H-T1 values of H3′, H5′, H1″ and H4″ decreased
Publikováno v:
Tetrahedron Letters. 48:5213-5217
Introduction of carbohydrate auxiliary into enanine-based catalyst provided a novel enantiocontrol for aqueous aldol reaction. Methyl 2-( l -prolyl)amido-2-deoxy-α- d -glucopyranosides led to the enantiocontrol as parent amino acids did in the react
Publikováno v:
Magnetic Resonance in Chemistry. 45:518-521
Structural elucidation of a malate-aluminum(III) complex has been carried out using 1H and 27Al NMR spectroscopy. The 1H chemical shift perturbation clearly indicated the interaction between malate and Al(III) ion. The measurements of 27Al NMR and 1H
Publikováno v:
Journal of Carbohydrate Chemistry. 25:521-532
The crystal structure of α,α‐trehalose hydrate complexed with calcium chloride was determined by X‐ray crystallography and its structural comparison with the α,α‐trehalose–CaBr2 · H2O complex was performed. The crystal system of the α,