Zobrazeno 1 - 6
of 6
pro vyhledávání: '"Tom Catalano"'
Publikováno v:
Journal of Pharmaceutical and Biomedical Analysis. 26:725-738
Assay development, assay validation, and documentation are reported here for a single packed column pressurized fluid chromatographic/ultraviolet (UV) method that provides: (1) simultaneous detection and quantification for the chiral drug, the chiral
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::c9f12f885639690f4af6333082b1d037
https://doi.org/10.1016/s0731-7085(01)00441-1
https://doi.org/10.1016/s0731-7085(01)00441-1
Publikováno v:
Journal of Chromatography A. 887:347-365
Various parameters have been evaluated to develop a process for optimization of column manufacture for packed capillary electrochromatography (CEC). Spherisorb ODS-1 was packed into 75 microm I.D. capillaries to establish a standard set of packing co
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::be1ad129da05fa9bcc05259d5f0ce11b
https://doi.org/10.1016/s0021-9673(00)00529-x
https://doi.org/10.1016/s0021-9673(00)00529-x
Publikováno v:
Electrophoresis. 20:2349-2359
Reversed-phase nonporous silica (RP-NPS) of 1.5 microm dp is employed to demonstrate rapid and efficient separations in packed capillary electrochromatography (CEC). Two methods for packing capillaries and two techniques to manufacture frits used to
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::6badc7f8981c63c4955706c4e746bb19
https://doi.org/10.1002/(sici)1522-2683(19990801)20:12<2349::aid-elps2349>3.0.co
https://doi.org/10.1002/(sici)1522-2683(19990801)20:12<2349::aid-elps2349>3.0.co
Publikováno v:
Journal of Chromatography A. 588:187-193
An ion-pairing high-performance liquid chromatographic method has been developed for the determination of 5-aminosalicylic acid (5-ASA) bulk chemical in the presence of thirteen potential synthetic process impurities. In addition, the method is suita
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::6e060000d8defa7eece24e826ef90a2f
https://doi.org/10.1016/0021-9673(91)85022-8
https://doi.org/10.1016/0021-9673(91)85022-8
Publikováno v:
Journal of pharmaceutical and biomedical analysis. 26(3)
The current study assesses the effect of extending column length during gradient packed column sub/supercritical fluid chromatography (PCSFC) experiments on the detection of known and unknown impurities in a drug substance sample. Quantitative drug s
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::1ef17dcb123fc72de170d8a33782ebef
https://pubmed.ncbi.nlm.nih.gov/11489380
https://pubmed.ncbi.nlm.nih.gov/11489380
Autor:
Estelita Victorino, Kent M. Payne, Tom Catalano, John F. Stobaugh, Peter D. A. Angus, Charles W. Demarest
Publikováno v:
Electrophoresis. 19(12)
Capillary electrochromatography (CEC) has been employed to explore method development for a series of structurally related polar neutral compounds of pharmaceutical relevance. Capillaries with dimensions of 75 microm ID x 25 cm length (34.5 cm total)
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::cced1a266b1d9de85ebbba1af073faca
https://pubmed.ncbi.nlm.nih.gov/9761184
https://pubmed.ncbi.nlm.nih.gov/9761184