Zobrazeno 1 - 10
of 15
pro vyhledávání: '"Tom Benijts"'
Publikováno v:
Journal of Chromatography A. 1029:153-159
In recent years, despite the increasing success of liquid chromatography (LC) coupled to tandem mass spectrometry (MS), reports on matrix susceptibility have shown the limitations of the this powerful analytical technique. Matrix effects (MEs) result
Publikováno v:
Analytical Chemistry. 76:704-711
An analytical method for the determination of 35 endocrine disrupting chemicals (EDCs) present in the aquatic environment was developed and validated. The procedure includes an off-line solid-phase extraction of 500-mL water samples using wide-spectr
Publikováno v:
Rapid Communications in Mass Spectrometry. 17:1866-1872
A sonic spray ionization liquid chromatography/mass spectrometry (LC/SSI-MS) procedure combined with off-line solid-phase extraction was optimized for the analysis of 20 endocrine-disrupting chemicals (EDCs) in water samples. Method development inclu
Autor:
D. Borrey, Willy E. Lambert, C. Van Peteghem, E. A. De Letter, Tom Benijts, A.P. De Leenheer, Michel Piette
Publikováno v:
Journal of Analytical Toxicology. 27:47-52
A few days after her admittance to a hospital for a suicide attempt with benzodiazepines, a 15-year-old girl was found dead in bed. At autopsy, no specific anatomo-pathologic cause of death was identified. Systematic toxicological analysis (HPLC-DAD,
Publikováno v:
Rapid Communications in Mass Spectrometry. 16:1358-1364
A precise and reliable method, using liquid chromatography combined with ion trap based mass spectrometry, for the determination of three endogenous estrogens, namely, estrone, estradiol, and estriol, and two synthetic estrogens, ethinyl estradiol an
Publikováno v:
Journal of Chromatography B. 773:53-61
A fast liquid chromatographic method with tandem diode array–fluorescence detection for the simultaneous determination of in total 17 opium alkaloids and opioids is presented. Blank blood and urine samples (1 ml) were spiked with different concentr
Publikováno v:
Analytical Chemistry. 74:3206-3212
Sonic spray (SS) ionization is a relatively novel atmospheric pressure ionization technique for LC/MS, based on the principle of "spray ionization", which only recently became commercially available. In this paper, we evaluate the performance of this
Publikováno v:
Rapid Communications in Mass Spectrometry. 16:1072-1077
A comparative study of three atmospheric-pressure ionization (API) sources for liquid chromatography/mass spectrometry (LC/MS), namely pneumatically assisted electrospray or ionspray (IS), atmospheric-pressure chemical ionization (APCI), and sonic sp
Publikováno v:
Journal of pharmaceutical and biomedical analysis. 32(4-5)
Stir bar sorptive extraction (SBSE) in combination with thermal desorption (TD) on-line coupled to capillary gas chromatography–mass spectrometry (CGC–MS) was applied to the analysis of pharmaceutical drug compounds and metabolites in urine. SBSE
Publikováno v:
Rapid communications in mass spectrometry : RCM. 17(16)
A sonic spray ionization liquid chromatography/mass spectrometry (LC/SSI-MS) procedure combined with off-line solid-phase extraction was optimized for the analysis of 20 endocrine-disrupting chemicals (EDCs) in water samples. Method development inclu