Zobrazeno 1 - 10
of 795
pro vyhledávání: '"Thomas Schleid"'
Publikováno v:
IUCrData, Vol 9, Iss 9, p x240888 (2024)
The title compound, diytterbium enneaoxidotritellurate(IV), was obtained in its C-type crystal structure from the binary oxides at 1073 K using a CsCl flux. It crystallizes isotypically with C-type Tm2Te3O9 and Lu2Te3O9, closing this gap of knowledge
Externí odkaz:
https://doaj.org/article/f05870860d2d4a1cb55b583947a9bc2f
Publikováno v:
Frontiers in Chemistry, Vol 12 (2024)
The multi-anionic compound with the composition Dy36O11F50[AsO3]12 ∙ H2O, which can be described in the non-centrosymmetric cubic space group F4¯3c, already shows an unusually large unit cell with an axis of a = 2587.59(14) pm. Its crystal structu
Externí odkaz:
https://doaj.org/article/0dbb70d22727487b8955bd7a86b6e541
Publikováno v:
IUCrData, Vol 8, Iss 8, p x230654 (2023)
The title compound, digadolinium(III) oxidodisilicate, Gd2[Si2O7], was obtained in its M-type crystal structure after attempts to synthesize Gd5Br3[AsO3]4 as a by-product from fused silica ampoules. It crystallizes isotypically with M-type Eu2[Si2O7]
Externí odkaz:
https://doaj.org/article/07f2b4fb427a4f409bf4d7783e2a0141
Publikováno v:
Crystals, Vol 14, Iss 4, p 310 (2024)
Two novel energetic anti-perovskite compounds with the chemical formula (N2H5)3X[B12H12] · H2O, where X− is either [NO3]− or [ClO4]−, were successfully synthesized. Both dodecahydro-closo-dodecaborates crystallize orthorhombically in the space
Externí odkaz:
https://doaj.org/article/f7546f04e10249f99fef95fe92b978c3
Publikováno v:
IUCrData, Vol 8, Iss 7, p x230591 (2023)
The title compound, dicerium(III) oxidodisilicate, Ce2[Si2O7], was obtained as a by-product in its H-type structure after attempts to synthesize CeSb2O4Cl from fused silica ampoules. It crystallizes isotypically with H-La2[Si2O7]. The four crystallog
Externí odkaz:
https://doaj.org/article/bcc42c909aa3452aa8e5362f23f4a44c
Publikováno v:
Molecules, Vol 29, Iss 2, p 382 (2024)
Three novel anti-perovskite compounds, formulated as Cs3X[B12H12] (X− = [NO3]−, [ClO3]−, and [ClO4]−), were successfully synthesized through the direct mixing of aqueous solutions containing Cs2[B12H12] and CsX (X−: [NO3]−, [ClO3]−, [Cl
Externí odkaz:
https://doaj.org/article/d2edfbf328434a44b26771c90d32af00
Autor:
Katja Engel, Thomas Schleid
Publikováno v:
Inorganics, Vol 11, Iss 12, p 465 (2023)
The new rubidium-containing erbium sulfide thioarsenate(III) with the structured formula RbEr2S(S2)[AsS2(S2)] was obtained from the syntheses of elemental erbium (Er), arsenic sesquisulfide (As2S3) and rubidium sesquisulfide (Rb2S3) with elemental su
Externí odkaz:
https://doaj.org/article/15dfcf756da3460daf687a11e34ec816
Publikováno v:
Crystals, Vol 13, Iss 10, p 1408 (2023)
The synthesis and structural analysis of three new chloride-containing lithium thiophosphates(V) Li4Ln[PS4]2Cl with trivalent lanthanoids (Ln = Pr, Nd and Sm) are presented and discussed. Single crystals of Li4Sm[PS4]2Cl were obtained and used for cr
Externí odkaz:
https://doaj.org/article/5436b6a48db948c3880f9b641b9a27af
Publikováno v:
Crystals, Vol 13, Iss 5, p 731 (2023)
It was possible to synthesize colorless single crystals of La5Cl3[SbO3]4 (block-shaped) as well as La2Sb12O19Br4 and La2Sb12O19I4 (both needle-shaped), representing three new compounds from the system of lanthanum oxoantimonate(III) halides, which ha
Externí odkaz:
https://doaj.org/article/e2200bb59dcc47c5be3da1897ed1240e
Autor:
Marion C. Schäfer, Michael Petter, Ingo Hartenbach, Ralf J. C. Locke, Shuang Zhang, Claudia Wickleder, Thomas Schleid
Publikováno v:
Crystals, Vol 13, Iss 3, p 511 (2023)
With Tm3F[Si3O10], a new representative of the Ln3F[Si3O10] series could be synthesized by the reaction of Tm2O3, TmF3 and SiO2 (molar ratio: 1:1:3), applying an excess of CsBr as a fluxing agent in gas-tightly sealed platinum crucibles for eight day
Externí odkaz:
https://doaj.org/article/bad0940ab5564442909c78dcedff33f6