Zobrazeno 1 - 10
of 22
pro vyhledávání: '"Tadashi Yonemitsu"'
Autor:
Shin-ichiro Isobe, Tadashi Yonemitsu, Thies Thiemann, Shuntaro Mataka, Tsuyoshi Sawada, Kanji Kubo
Publikováno v:
Bulletin of the Chemical Society of Japan. 75:773-779
Arylhydroxymethano[3]orthocyclo[5](1,8)naphthalenophanes 11, which possess a rigid boat-chair conformation, were prepared by the reaction of 9,10-benzo-3,4,5-[1,8]naphthobicyclo[5.4.1]dodecan-3,9-dien-12-one 8c with aryllithium reagents and treated w
Publikováno v:
Phosphorus, Sulfur, and Silicon and the Related Elements. 167:239-249
High purity synthesis of ω-ferrocenylalkanethiols (Fc(CH2)n−SH, n=6, 8, 11) was developed for their use in self-assembled monolayers on gold surface. The method employs a separation and purification of isothiuronium salt 6 to improve the purity of
Autor:
Kichinosuke Kamata, kuniharu Takahashi, Akira Kitamura, Masashi Tashiro, Gouki Fukata, Akiyoshi Torii, Tadashi Yonemitsu, Shuntaro Mataka
Publikováno v:
food preservation science. 25:105-110
The entire series of 9-straight chain alkylated acridine derivatives which are acridine (1, C0) -9-n-octiylacridine (9, C8) except C0 were synthesized and C0 was purchased. The relationship between the number of carbon chains on 9-straight chain alky
Autor:
Masahiko Taniguchi, Shin-ichiro Isobe, Shuntaro Mataka, Thies Thiemann, Tsuyoshi Sawada, Tadashi Yonemitsu
Publikováno v:
Journal of the Chemical Society, Perkin Transactions 1. :2101-2108
Novel rearrangement of intermediate carbocations generated from rigid, layered [3.3]orthocyclophane-alcohols 4 are presented. The bicyclo[4.4.1]undecane framework of 4 rearranges to either bicyclo[5.4.0]- 5 and/or bicyclo[4.4.0]- 6 or tricyclo[5.4.0.
Autor:
Takehito Tsukinoki, Masashi Tashiro, Yoshiaki Nagano, Tadashi Yonemitsu, M. Mukumoto, Hirohisa Tsuzuki, Shuntaro Mataka
Publikováno v:
Journal of Labelled Compounds and Radiopharmaceuticals. 34:1087-1090
[2H13]Heptanoic acid was synthesized as its methyl ester (4) (deuterium content: 96%) with Ni-Al alloy in 10% NaOD-D2O via the desulfurization of methyl 3-chloro-5,6-dibromothieno[3,2,b]thiophene-2-carboxylate (3), which was derived from 4,5-dibromot
Autor:
Katsuhiko Kamio, Hirohisa Tsuzuki, Hideki Fujimoto, Keisuke Mimura, Susumu Matsumoto, Tadashi Yonemitsu, Shuntaro Mataka, Masashi Tashiro, Takehito Tsukinoki
Publikováno v:
Journal of Labelled Compounds and Radiopharmaceuticals. 33:205-212
The synthesis of [4,5,6,8-2H4][2.2]metacyclophane (8) was achieved starting with 2,4,5,6-tetrafluoroisophthalic acid in eight steps in 2% total yield. 1H{2H} and 13C{1H} NMR spectra of 8 showed that the deuterium atoms were introduced at the desired
Autor:
Thies Thiemann, Shuntaro Mataka, Tadashi Yonemitsu, Masahiko Taniguchi, Shin-ichiro Isobe, Tsuyoshi Sawada
Publikováno v:
ChemInform. 30
Novel rearrangement of intermediate carbocations generated from rigid, layered [3.3]orthocyclophane-alcohols 4 are presented. The bicyclo[4.4.1]undecane framework of 4 rearranges to either bicyclo[5.4.0]- 5 and/or bicyclo[4.4.0]- 6 or tricyclo[5.4.0.
Publikováno v:
Bulletin of the Chemical Society of Japan. 64:3094-3097
The proton NMR spectra of 1-tetradecanesulfonates whose cationic counterion, the 1,1′-polymethylenedipyridinium ion (with even-numbered methylene groups up to 14), is divalent with separate electric charge, were measured. From the chemical shifts t
Publikováno v:
Journal of Labelled Compounds and Radiopharmaceuticals. 29:691-701
[2-2H1]-, [2,3-2H2]-, [2,2,3-2H3]-, and [4,4,5,5,5-2H5]Valeric acids, and trans- and cis-2-[2-2H1]pentenoic acid and 4-[4,5,5-2H3]pentenoic acid have been synthesized from 2-bromovaleric acid, trans-2-pentenoic acid, 2,3-dibromovaleric acid, and 4-pe
Autor:
Masashi Tashiro, Hirohisa Tsuzuki, Tadashi Yonemitsu, Shin-ichiro Isobe, Shoji Ogasahara, Hideyuki Goto, Shuntaro Mataka
Publikováno v:
Journal of Labelled Compounds and Radiopharmaceuticals. 29:405-414
Succinic [2,3-2H2]- and [2,2,3,3-2H4]-acids were prepared from maleic anhydride and dimethyl fumarate, and acetylene dicarboxylic acid and its dimethyl ester by treatment with CuAl and Ni-Al alloys in 10% NaOD-D2O in 95% to 100% isotopic purity. The