Zobrazeno 1 - 5
of 5
pro vyhledávání: '"T. Michael Barnard"'
Publikováno v:
Energy & Fuels. 22:2005-2008
The batch and continuous-flow preparation of biodiesel derived from vegetable oil and 1-butanol using a commercially available scientific microwave apparatus is reported. The methodology allows for the reaction to be run under atmospheric conditions
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::e747073e0936e7edca9e986feaea45a0
https://doi.org/10.1021/ef700748t
https://doi.org/10.1021/ef700748t
Publikováno v:
Tetrahedron Letters. 49:195-198
By interfacing a digital camera with a scientific microwave unit it is possible to monitor macroscopic effects as reactions proceed, including color and viscosity changes, evolution of gases, metal-mediated couplings, and arcing.
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::e9316eca63975006235dc47c30ec8dfd
https://doi.org/10.1016/j.tetlet.2007.10.097
https://doi.org/10.1016/j.tetlet.2007.10.097
Autor:
Matthew B. Boucher, Lauren M. Stencel, Benjamin A. Wilhite, T. Michael Barnard, Nicholas E. Leadbeater
Publikováno v:
Energy & Fuels. 21:1777-1781
The continuous-flow preparation of biodiesel using a commercially available scientific microwave apparatus offers a fast, easy route to this valuable biofuel. The methodology allows for the reaction to be run under atmospheric conditions and performe
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::76864f8659ad5a14f6b5260ecd360419
https://doi.org/10.1021/ef0606207
https://doi.org/10.1021/ef0606207
Publikováno v:
Organic Process Research & Development. 10:1233-1237
A green approach to N-heterocyclization reactions ranging in scale from 20 mmol to 1 mol performed under microwave irradiation in open vessels has been investigated. By using water as the solvent and no transition metal catalysts, N-heterocycles are
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::3245b35453564fa6798694809a380520
https://doi.org/10.1021/op0601722
https://doi.org/10.1021/op0601722
Publikováno v:
Organicbiomolecular chemistry. 5(5)
Microwave-promoted esterification reactions have been monitored using in situ Raman spectroscopy. Having optimised a reaction on a 23 mmol scale, it was transferred to a larger reaction vessel and scaled up to 0.26 mol, again with Raman monitoring. W
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::5946711865171c49d8a19735d2bc042c
https://pubmed.ncbi.nlm.nih.gov/17315069
https://pubmed.ncbi.nlm.nih.gov/17315069