Zobrazeno 1 - 10 of 16 pro vyhledávání: '"Susanne Margot Rupf"'
1
Increasing the oxidation power of TCNQ by coordination of B(C6F5)3
Autor: Paul Anton Albrecht, Susanne Margot Rupf, Malte Sellin, Johanna Schlögl, Sebastian Riedel, Moritz Malischewski
Publikováno v: Chemical Communications. 58:4958-4961
A mixture of TCNQ and four equivalents of B(C6F5)3 is strongly oxidizing and readily forms the new weakly-coordinating anions [TCNQ·4 B(C6F5)3]− and [TCNQ·4 B(C6F5)3]2−.
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::046c4ab6a652a58964b5b4a40080925b
https://doi.org/10.1039/d2cc00314g
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2
Structural Characterization and Bonding Analysis of [Hg{Fe(CO)5}2]2+ [SbF6]-2
Autor: Susanne Margot Rupf, Sudip Pan, Amina Leoni Moshtaha, Gernot Frenking, Moritz Malischewski
The non-classical carbonyl complex [Hg{Fe(CO)5}2]2+ [SbF6]-2 is prepared by reaction of Hg(SbF6)2 and excess Fe(CO)5 in anhydrous HF. The single-crystal X-ray structure reveals a linear Fe-Hg-Fe moiety as well as an eclipsed conformation of the eight
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::8aa32609d040df4da97538ce29cfcec8
https://doi.org/10.26434/chemrxiv-2023-0tp5j
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3
A decacationic ferrocene-based metallostar
Autor: Susanne Margot Rupf, Amina Leoni Moshtaha, Moritz Malischewski
Decacationic metallostars have been prepared by the reaction of permercurated ferrocene FeC10(HgO2CCF3)10 with superacidic (C5F5NH)(SbF6) (pKa = −11 estimated in H2O) in multigram scale. In the resulting compound, [FeC10Hg10(NC5F5)n][SbF6]10, the l
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::f5bd57cc6c37725653fd2dba592f654c
https://doi.org/10.17169/refubium-37926
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4
On pyridine chloronium cations
Autor: Patrick Pröhm, Willi Berg, Susanne Margot Rupf, Carsten Müller, Sebastian Riedel
We present the first solid-state structural evidence of mono- and bis(pyridine)chloronium cations. The latter was synthesized from a mixture of pyridine, elemental chlorine and sodium tetrafluoroborate in propionitrile at low temperatures. The mono(p
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::0b08e517fca003888ff0d4ba6cc560a1
https://refubium.fu-berlin.de/handle/fub188/38853
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5
Investigation of Bis(Perfluoro‐ tert ‐Butoxy) Halogenates(I/III)
Autor: Susanne Margot Rupf, Patrick Voßnacker, Willi R. Berg, Sebastian Riedel, Patrick Pröhm
Publikováno v: Chemistry – A European Journal. 27:17676-17681
A systematic study of halogenate(I/III) anions with polyatomic ligands is presented. The bis(perfluoro-tert-butoxy) halogenates(I) [X(OC4 F9 )2 ]- , X=Cl, Br, I, of chlorine, bromine, and iodine are prepared as their tetraethylammonium salts and char
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::e80d28789ea1219df418cc2d53ba5ce7
https://doi.org/10.1002/chem.202103325
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7
Eightfold Electrophilic Methylation of Octacyanotungstate [W(CN)8]4–/3–: Preparation of Homoleptic, Eight-Coordinate Methyl Isocyanide Complexes [W(CNMe)8]4+/5+
Autor: Susanne Margot Rupf, Moritz Malischewski, Malte Sellin, Ulrich Abram
Publikováno v: Inorganic Chemistry. 60:5917-5924
Homoleptic eightfold coordinated methyl isocyanide complexes of W(IV) and W(V) have been prepared for the first time. The reaction of [NBu4]4[W(CN)8] with methyl triflate (MeOTf) gives [W(CNMe)8][O...
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::13f0f6a4d5c3f9a30a4b66e1c592cecb
https://doi.org/10.1021/acs.inorgchem.1c00326
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8
Tenfold Metalation of Ferrocene: Synthesis, Structures, and Metallophilic Interactions in FeC10(HgX)10
Autor: Robin Sievers, Gabriel Schröder, Moritz Malischewski, Susanne Margot Rupf
Publikováno v: Chemistry (Weinheim an Der Bergstrasse, Germany)
The permercuration of ferrocene was achieved by reacting ferrocene with 10 equivalents of mercury(II) butyrate Hg(O2CC3H7)2 in a facile one‐pot reaction in multi‐gram scale and high yields. The butyrate groups in FeC10(HgX)10 (X=O2CC3H7) can be e
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::9055a18076f710401525b76771cbbfe4
http://europepmc.org/articles/PMC8048484
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9
Bi- and Trifurcated Halogen Bonding M–C≡N···I in 1D, 2D, and 3D Supramolecular Network Structures of Co-Crystallized Diiodoacetylene C2I2 and Tetracyanonickelate [Ni(CN)4]2–
Autor: Moritz Malischewski, Susanne Margot Rupf, Malte Sellin, Yuyin Zhang
Publikováno v: Crystal Growth & Design. 20:7104-7110
The co-crystallization of square-planar tetracyanonickelate(II) [Ni(CN)4]2– with an excess of the strong halogen bond donor diiodoacetylene C2I2 in dichloromethane results in the formation of supra...
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::d297f423b1873947a567a3024a55b3b8
https://doi.org/10.1021/acs.cgd.0c01208
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10
The [2+2] cycloaddition product of perhalogenated cyclopentadienyl cations: structural characterization of salts of the [C10Cl10]2+ and [C10Br10]2+ dications
Autor: Moritz Malischewski, Susanne Margot Rupf, Patrick Pröhm
Publikováno v: Chemical Communications. 56:9834-9837
Instead of monomeric cyclopentadienyl cations, the low-temperature reaction of hexachloro- and hexabromocyclo-pentadiene (C5Cl6 and C5Br6) with powerful Lewis acids SbF5 and AsF5 in SO2ClF yields salts of perhalogenated dications [C10Cl10][Sb3F16]2 a
Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::891188fd017ac3063fd61c96c9c614b8
https://doi.org/10.1039/d0cc04226a
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