Zobrazeno 1 - 10
of 16
pro vyhledávání: '"Steven M. Pyle"'
Autor:
Alvin B. Marcus, Steven M. Pyle
Publikováno v:
International Journal of Environmental Analytical Chemistry. 76:17-29
Direct aqueous injection analysis (DAI) with gas chromatographic separation and ion trap mass spectral detection was used to analyze aqueous samples for μg/L levels of 54 volatile and semivolatile compounds, and problematic non-purgeables and non-ex
Autor:
Steven M. Pyle, Peter A. Gabele
Publikováno v:
Environmental Science & Technology. 34:368-372
Air and water pollutant emissions were measured from two 9.9 HP outboard engines: a two-stroke Evinrude and its four-stroke Honda counterpart. In addition to the measurement of regulated air pollutants, speciated organic pollutants and particulate ma
Publikováno v:
Environmental Science & Technology. 32:3213-3217
Soil extracts from five Superfund Contract Laboratory Program (CLP) laboratories were analyzed for organochlorine pesticides using gas chromatographic separation with ion trap mass spectrometric detection in both electron impact (GC/EIMS) and tandem
Publikováno v:
International Journal of Mass Spectrometry and Ion Processes. 173:27-39
Ab initio and density functional theory (DFT) calculations have been performed to determine the heats of reaction for the process C 16 H 10 + → C 10 H 2 + that takes place in an ion trap mass spectrometer. Comparisons have been made with the experi
Autor:
Ky D. Nichols, John A. Palasota, Conrad A. Kuharic, Stanley N. Deming, William H. Cole, Daniel C. Hillman, Steven M. Pyle, Patricia M. Fitzpatrick, John M. Nocerino, Michael A. Watson, Josephine M. Palasota, Eric L. Miller
Publikováno v:
Environmental Science & Technology. 30:204-213
Samples from a hazardous waste site contaminated with lead and cadmium were analyzed by four independent laboratories, each using a different technique: atomic absorption spectroscopy (AAS), X-ray fluorescence (XRF) spectroscopy, inductively coupled
Publikováno v:
Analytical Chemistry. 66:2521-2528
A direct-deposition Fourier transform infrared (FT-IR) system has been evaluated for applicability to gas chromatography (GC) and supercritical fluid chromatography (SFC) of environmental analytes. A 100-μm i.d. fused-silica transfer line was used f
Publikováno v:
Journal of Chromatographic Science. 29:339-344
Publikováno v:
Talanta. 69(2)
A new technique to analyze aqueous samples for nanograms per liter levels of volatile and semivolatile compounds using microextraction and thermal desorption into a gas chromatograph/ion trap mass spectrometer (GC/MS) is described. This method is inh
Autor:
Steven M. Pyle, Matthew M. Setty
Publikováno v:
Talanta. 38(10)
Supercritical fluid extraction (SFE) of sulfur-containing soils and sediments was hindered by deposition of elemental sulfur in the restrictor stopping the flow of carbon dioxide. It was found that a copper scavenger column placed after the sample ce
Autor:
Steven M. Pyle, Alvin B. Marcus
Publikováno v:
Journal of Mass Spectrometry. 32:897-898