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of 68
pro vyhledávání: '"Stephen J. Heyes,† and"'
The isotopically labelled amino-functionalised ferrocene derivatives FcCH2CH215NH2 and Fc′CH2CH2NH2[Fc = Fe(η-C5H5)(η-C5H4); Fc′= Fe(η-C5D5)(η-C5D4)] have been synthesized. Their hydrochloride salts and the lamellar intercalation compounds Mo
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https://ora.ox.ac.uk/objects/uuid:e576bc02-f6f7-483d-ad49-09bdfef988f2
https://ora.ox.ac.uk/objects/uuid:e576bc02-f6f7-483d-ad49-09bdfef988f2
Variable-temperature solid-state 2H NMR spectra have been recorded on microcrystalline samples of [Mo(η-C6D6)2], [Mo{η-C6D3(CD3)3-1,3,5} 2] and [ZrS2{Mo[η-C6D3(CD3) 3-1,3,5]2}0.15]. In the case of [Mo(η-C6D6)2] the spectra are invariant in the ra
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https://ora.ox.ac.uk/objects/uuid:c5c73232-5fad-4037-ad23-258e4b3ab2ff
https://ora.ox.ac.uk/objects/uuid:c5c73232-5fad-4037-ad23-258e4b3ab2ff
Solid state 2H NMR spectra of single crystal samples of CdPS3{Co(η-C5D5)2}0.4 indicate the co-existence of both Co(η-C5D5)2 and [Co(η-C5D5)2]+between the CdPS3layers; all the metallocene guest molecules reside in ordered domains within the ab-plan
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https://explore.openaire.eu/search/publication?articleId=doi_dedup___::dc00870996d9998e1f48f28b3098eeb6
https://doi.org/10.1039/c39950001657
https://doi.org/10.1039/c39950001657
Autor:
Susan J. Mason, Peter A. Turner, Jon Greenwood, John S. O. Evans, Stephen J. Heyes, Dermot O'Hare
The orientations of [Co(C5D5)2] + ions intercalated in the xerogel V2O5· 1.6H2O have been studied using solid-state 2H NMR spectroscopy. The cobaltocenium ions in microcrystalline samples of V 2O5{Co(C5D5)2} 0.2(H2O)0.5 are observed to be held rigid
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https://doi.org/10.1039/jm9950501383
https://doi.org/10.1039/jm9950501383
Autor:
Roberto Gobetto, Fabio Napolitano, Silvio Aime, Holly C. Canuto, Michele R. Chierotti, Admir Masic, Stephen J. Heyes
Publikováno v:
European Journal of Inorganic Chemistry. 2008:152-157
Variable-temperature 13C CPMAS NMR spectra of the metal–carbonyl complexes FeCp(CO)2X (where X = I, CH3) and Mo2Cp2(CO)6 included in β- or γ-cyclodextrin (CD) cavities were investigated in the temperature range 133 to 293 K. The motion of the gue
Autor:
Mark G. Moloney, Stephen J. Heyes, Jonathan E. H. Buston, Timothy D. W. Claridge, Maya Stevenson, Jeremy L. Bretherton
Publikováno v:
Magnetic Resonance in Chemistry. 39:68-76
207Pb NMR spectroscopy was used to investigate 20 lead(IV) tetracarboxylates both in solution and in the solid state by cross-polarization magic angle spinning (CP/MAS) NMR. There is generally good correlation between isotropic chemical shifts in the
Autor:
Stephen J. Heyes, Keith Prout, Andrew McDaid, Matthias A. Müller, Thierry Maris, Matthew J. Seaman, Christopher M. Dobson
Publikováno v:
Chemistry of Materials. 12:3561-3569
Variable-temperature single-crystal X-ray experiments have been performed on the thiourea pyridinium chloride, bromide, and iodide inclusion compounds. Two phases were found for the chloride, three for the bromide, and two for the iodide. As previous
Publikováno v:
Chemistry of Materials. 12:1314-1322
The deoxycholic acid inclusion complex (DCA) 2 :ferrocene (1) undergoes a gradual phase transition above ambient temperature, completed by ∼360 K. The phase transition is characterized by using single-crystal X-ray diffraction and 13 C CP/MAS NMR s
Autor:
Michaela Wendeler, Alison J. Edwards, Jamila Fattah, Christopher M. Dobson, Stephen J. Heyes,† and, J. Mark Twyman, Keith Prout
Publikováno v:
Journal of the American Chemical Society. 119:9793-9803
13C CP/MAS NMR spectra of the free acid of phenoxymethyl penicillin (penicillin V) and of its lithium, sodium, rubidium, and cesium salts (C16H17N2O5SM, M = H, Li·H2O, Na, Rb, and Cs) have been studied at a range of temperatures between 180 and 400