Zobrazeno 1 - 10
of 10
pro vyhledávání: '"Stephan Dusold"'
Autor:
Stephan Dusold, Angelika Sebald, Matthias Bechmann, Jeremy N.S. Evans, Dan J. Mitchell, David L. Jakeman, Wendy A. Shuttleworth
Publikováno v:
Solid State Sciences. 6:1097-1105
The absolute orientations of the three 13 C chemical shielding tensors in the phosphoenolpyruvate (PEP) moiety in a PEP-model compound with known crystal structure are reported. The study uses a fully 13 C-enriched polycrystalline sample of triammoni
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::41102903f6446deb6c75ce90a2913683
https://doi.org/10.1016/j.solidstatesciences.2004.04.021
https://doi.org/10.1016/j.solidstatesciences.2004.04.021
Autor:
Stephan Dusold, Angelika Sebald
Publikováno v:
Journal of Magnetic Resonance. 145:340-356
The dependence of the performance of a recently introduced pulse sequence to achieve double-quantum excitation under the n = 1 rotational-resonance condition (T. Karlsson, M. Eden, H. Luthman, and M. H. Levitt, 2000, J. Magn. Reson. 145, 95-107) on d
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::ee3c931c07574a3af0e577f4e9770f9d
https://doi.org/10.1006/jmre.2000.2118
https://doi.org/10.1006/jmre.2000.2118
Autor:
Stephan Dusold, Angelika Sebald
Publikováno v:
Molecular Physics. 95:1237-1245
Possibilities and limitations for the complete determination of all orientational parameters from iterative fitting of various MAS NMR spectra of ABX three-spin systems are explored. The practical example chosen is the (31P)2 113Cd ABX spin system in
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::402999b476e9308155d960b96d334645
https://doi.org/10.1080/00268979809483254
https://doi.org/10.1080/00268979809483254
Publikováno v:
The Journal of Physical Chemistry B. 101:6359-6366
Two-dimensional 31P spin diffusion MAS NMR experiments on polycrystalline Cd3(PO4)2, using a broad-banded dipolar recoupling scheme, are reported. Quantitative analysis of the 31P spin diffusion experiments as a function of mixing times yields unambi
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::6cee395e8ae7db98233dc95e95431199
https://doi.org/10.1021/jp9709924
https://doi.org/10.1021/jp9709924
Publikováno v:
Journal of the American Chemical Society. 119:7121-7129
Accurate measurements of the magnitudes and relative orientations of chemical shielding, J coupling and dipolar coupling tensors for isolated homonuclear 31P−31P spin pairs, using standard 31P MAS ...
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::ae5ed9a17ea84f75bac738872ec36ccb
https://doi.org/10.1021/ja970890r
https://doi.org/10.1021/ja970890r
Publikováno v:
The journal of physical chemistry. A. 109(24)
31P MAS and double-quantum filtered 31P MAS NMR experiments at and near the n = 0 rotational resonance condition, as well as off-magic angle spinning 31P NMR experiments on two polycrystalline samples of Pt(II)−phosphine thiolate complexes are repo
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::6ed8c66e59bcf32628d0d5d47c351fae
https://pubmed.ncbi.nlm.nih.gov/16839050
https://pubmed.ncbi.nlm.nih.gov/16839050
Autor:
Angelika Sebald, Hans Förster, Ulrich Haeberlen, Stephan Dusold, Matthias Bechmann, Tadeusz Lis, Michael Stumber
Publikováno v:
Molecular Physics
A 31P and 13C NMR study of powder and single crystal samples of two phosphoenolpyruvate (PEP) compounds, the tris-ammonium salt monohydrate (NH4)3(PEP)·H2O (1), and the mono-ammonium-salt (NH4)(H2PEP) (2) is presented. The P chemical shielding tenso
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::df492be896360d9bc57e1844f24f4d52
https://hdl.handle.net/11858/00-001M-0000-0028-3558-111858/00-001M-0000-0028-3556-5
https://hdl.handle.net/11858/00-001M-0000-0028-3558-111858/00-001M-0000-0028-3556-5
Autor:
Angelika Sebald, Stephan Dusold
Experimental NMR techniques designed to recouple weak homonuclear and heteronuclear dipolar coupling interactions under magic-angle spinning conditions are discussed. Developments and applications of such dipolar recoupling techniques are reviewed, c
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::f6a3292d31bb01f21774349e61eeddd8
https://doi.org/10.1016/s0066-4103(00)41010-0
https://doi.org/10.1016/s0066-4103(00)41010-0
Publikováno v:
Journal of magnetic resonance (San Diego, Calif. : 1997). 141(1)
Possibilities and limitations of iterative lineshape fitting approaches for the complete determination of magnitudes and orientations of NMR interaction tensors in a four-(13)C-spin system from MAS NMR experiments are investigated. The availability o
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::0782cf29e5645a7e48386d16c7f6590d
https://pubmed.ncbi.nlm.nih.gov/10527746
https://pubmed.ncbi.nlm.nih.gov/10527746
Publikováno v:
Journal of magnetic resonance (San Diego, Calif. : 1997). 135(2)
Possibilities and limitations of iterative lineshape fitting procedures of MAS NMR spectra of isolated homonuclear spin pairs, aiming at determination of magnitudes and orientations of the various interaction tensors, are explored. Requirements regar
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::3a99f594e18d1177d31d1f4250159bdd
https://pubmed.ncbi.nlm.nih.gov/9878477
https://pubmed.ncbi.nlm.nih.gov/9878477