Zobrazeno 1 - 10
of 81
pro vyhledávání: '"Stan A. Duraj"'
Autor:
Robert Alan Woloszynek, Aloysius F. Hepp, John D. Protasiewicz, Michael Q. Dequeant, Stan A. Duraj, Tong Ren
Publikováno v:
Inorganica Chimica Acta. 365:54-60
Two new heteroleptic chelated-benzoato gallium (III) and indium (III) complexes have been prepared and structurally characterized. The molecular structures of [GaCl2(4-Mepy)2(O2CPh)]·4-Mepy (1) and [InCl(4-Mepy)2(O2CPh)2]·4-Mepy (2) have been deter
Publikováno v:
Journal of Thermal Analysis and Calorimetry. 75:929-935
A family of single source precursors, for the spray chemical vapor deposition (CVD) of chalcopyrite thin films (CuInS2), has been synthesized in good yields (ca. 65%). Newly synthesized compounds include [{L}2Cu(SR)2In(SR)2], (R=alkyl, aryl; L=neutra
Publikováno v:
Journal of Coordination Chemistry. 56:647-653
Publikováno v:
Journal of Coordination Chemistry. 56:307-312
The synthesis and structural characterization of a novel ionic Ga(III) five coordinate complex [{CH3(C5H4N)}Ga(SCH2(CO)O)2]-[(4-MepyH)]+, (4-Mepy = CH3(C5H5N)) from the reaction between Ga2Cl4 with sodium mercapto-acetic acid in 4-methylpyridine is d
Publikováno v:
Inorganica Chimica Acta. 338:99-104
Three new isothiocyanate-4-methylpyridine anionic compounds were prepared by refluxing metal powders (Mn, Fe, and Cu) with thiourea in 4-methylpyridine (γ-picoline). The isothiocyanate ligand is believed to be generated in situ by the isomerization
Autor:
Kulbinder K. Banger, Philip E. Fanwick, Aloysius F. Hepp, Stan A. Duraj, Robert A. Martuch, David G. Hehemann
Publikováno v:
Journal of Coordination Chemistry. 55:1427-1431
The synthesis and structural characterization of a novel In(III) complex is described. The reaction between InCl3 with sodium mercapto-acetic acid, (NaSCH2(CO)OH) in 4-methylpyridine, (CH3(C5H5N), (4-Mepy)) at 25 C affords [ClIn(SCH2(CO)O)2]2- [(4-Me
Publikováno v:
Journal of Coordination Chemistry. 55:1045-1051
The crystal and molecular structure of the title compound, VOCl(O2CCH3)(4-CH3C5H4N)2, has been determined by single-crystal x-ray diffraction. The material crystallizes in the space group P 1(bar) (#2) with a = 7.822(2), b = 8.023(l), c = 14.841(2) A
Autor:
Jerry D. Harris, John F. Richardson, Phillip E. Fanwick, Stan A. Duraj, Aloysius F. Hepp, William E. Eckles, Edward M. Gordon
Publikováno v:
Materials & Design. 22:625-634
A new synthetic route to isothiocyanate containing materials is presented. Five isothiocyanate 4-methylpyridine (γ-picoline) compounds were prepared by refluxing metal powders (Fe, Co, Ni and Cu) with thiourea in γ-picoline. The isothiocyanate liga
Publikováno v:
Journal of Coordination Chemistry. 52:111-117
The synthesis and structure of the indium dithiocarbamate, In[S2CN(CH3)2]30 central dot 1/2 4- mepy (4-mepy = 4-methylpyridine), is described. Indium metal was oxidized by tetramethylthiuramdisulfide in 4-methylpyridine at 25 C to form a new, homolep
Autor:
Aloysius F. Hepp, John D. Schupp, Stan A. Duraj, Shawn Long, Edward M. Gordon, William E. Eckles, Tuhfeh S. Habash, Phillip E. Fanwick
Publikováno v:
Inorganica Chimica Acta. 257:247-251
The three compounds Ga2Cl4(4-mepy)2 (1),[GaCl2(4-mepy)4]GaCl4x1/2(4-mepy); (2) and GaCl2(4-mepy)2(S2CNEt2); (3) (4-mepy= 4-methylpyridine) have been prepared from reactions of gallium (II) chloride in 4-methylpyridine and characterized by single-crys