Zobrazeno 1 - 10
of 15
pro vyhledávání: '"Sini, Panicker"'
Publikováno v:
Drug Testing and Analysis. 14:505-513
The forensic analysis of stable isotopes is a valuable tool to geo-source natural or semisynthetic drugs such as cocaine and heroin. The present study describes a novel methodology to isolate morphine from opium for isotopic analysis. Furthermore, th
Publikováno v:
Scientific Reports, Vol 8, Iss 1, Pp 1-15 (2018)
Scientific Reports
Scientific Reports
This study is the first to report the successful development of a method to extract opium poppy (Papaver somniferum L.) DNA from heroin samples. Determining of the source of an unknown heroin sample (forensic geosourcing) is vital to informing domest
Publikováno v:
Inorganica Chimica Acta. 468:294-299
Heroin manufacturing and distribution by criminal and terrorist organizations produce illicit economic benefits from the opium and heroin trade and result in devastating societal problems. Heroin chemical signatures provide important information to l
Publikováno v:
Drug testing and analysis. 11(7)
Porphyroxine, a trace alkaloid in opium, was identified in the early 1800s and isolated/characterized in the 1960s. Recently, two significant porphyroxine-related byproducts found in the acidic and neutral extracts of illicit heroin were characterize
Publikováno v:
Drug Testing and Analysis. 9:462-469
Two significant compounds often found in the gas chromatographic analysis of the acid/neutral extracts from illicit heroin have remained uncharacterized for 30 years. The unknown compounds are referred to as the 'B' and 'C' compounds. It has been pos
Publikováno v:
Drug testing and analysis. 9(3)
Two significant compounds often found in the gas chromatographic analysis of the acid/neutral extracts from illicit heroin have remained uncharacterized for 30 years. The unknown compounds are referred to as the 'B' and 'C' compounds. It has been pos
Publikováno v:
Journal of Chromatography A. 1034:227-235
Rapid, precise, accurate, and reproducible methodology using capillary electrophoresis (CE) with dynamically coated capillaries for the analysis of heroin and its basic impurities and adulterants is presented. Highly selective determination of the ab
Publikováno v:
Journal of Chromatography A. 984:109-120
A rapid, precise, accurate, and robust method using capillary electrophoresis (CE) with dynamically coated capillaries for the analysis of the major opium alkaloids in opium is presented. Dynamic coating of the capillary surface is accomplished using
Publikováno v:
Forensic science international. 231(1-3)
Rapid, precise, accurate, and reproducible methodology using ultra-high-pressure liquid chromatography (UHPLC) for the analysis of heroin and basic impurities is described. The determination of heroin, morphine, O3-monoacetylmorphine, O6-monoacetylmo
Autor:
Sini Panicker, Jerome A. Klun, Jesse M. Nicholson, Rolland M. Waters, Achot P. Khrimian, James E. Oliver
Publikováno v:
Tetrahedron: Asymmetry. 7:37-40
Chiral syntheses of 2-fluoro carboxylic acids were achieved (ee ≥ 92%, yield 50–60%) by stereoselective conversion (with inversion of configuration) of optically active trichloromethyl carbinols to fluoroacids with tetrabutylammonium fluoride. Fl