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Cryogen-free 400-MHz nuclear magnetic resonance spectrometer as a versatile tool for pharmaceutical process analytical technology.

Autor: Silva Elipe MV; Department of Attribute Sciences, Process Development, Amgen Inc., Thousand Oaks, California, USA., Ndukwe IE; Department of Attribute Sciences, Process Development, Amgen Inc., Thousand Oaks, California, USA., Murray JI; Pivotal and Commercial Drug Substance Technologies, Process Development, Amgen Inc., Thousand Oaks, California, USA.

Publikováno v: Magnetic resonance in chemistry : MRC [Magn Reson Chem] 2024 Jul; Vol. 62 (7), pp. 512-534. Date of Electronic Publication: 2024 Feb 18.

Atroposelective Brønsted Acid-Catalyzed Photocyclization to Access Chiral N -Aryl Quinolones with Low Rotational Barriers.

Autor: Arunachalampillai A; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Chandrappa P; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Cherney A; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Crockett R; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Doerfler J; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Johnson G; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Kommuri VC; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Kyad A; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., McManus J; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Murray J; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Myren T; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Fine Nathel N; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Ndukwe I; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Ortiz A; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Reed M; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Rui H; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Silva Elipe MV; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Tedrow J; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Wells S; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Yacoob S; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States., Yamamoto K; Amgen, One Amgen Center Drive, Thousand Oaks, California 91320, United States.

Publikováno v: Organic letters [Org Lett] 2023 Aug 11; Vol. 25 (31), pp. 5856-5861. Date of Electronic Publication: 2023 Jul 27.

An algorithm for discovery and determination of exponentially decaying components in nuclear magnetic resonance relaxometry data.

Autor: Ponte S; Development Department, Mestrelab Research S.L., Santiago de Compostela, Spain., Silva Elipe MV; Department of Attribute Sciences, Amgen Inc., Thousand Oaks, CA, USA., Aboutanios E; School of Electrical Engineering and Telecommunications, UNSW Sidney, Sydney, Australia., Vasini EM; Management, Extra Byte snc, Castano Primo, MI, Italy., Cobas C; Development Department, Mestrelab Research S.L., Santiago de Compostela, Spain.

Publikováno v: Magnetic resonance in chemistry : MRC [Magn Reson Chem] 2019 Aug; Vol. 57 (10), pp. 878-899.

Development of a Commercial Process To Prepare AMG 232 Using a Green Ozonolysis-Pinnick Tandem Transformation.

Autor: Cochran BM; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Corbett MT; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Correll TL; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Fang YQ; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Flick TG; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Jones SC; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Silva Elipe MV; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Smith AG; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Tucker JL; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Vounatsos F; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Wells G; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Yeung D; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Walker SD; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Bio MM; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States., Caille S; Pivotal Drug Substance Technologies , Amgen Inc ., One Amgen Center Drive , Thousand Oaks , California 91320 , United States.

Publikováno v: The Journal of organic chemistry [J Org Chem] 2019 Apr 19; Vol. 84 (8), pp. 4763-4779. Date of Electronic Publication: 2019 Jan 02.